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Date submitted2023-10-02
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Date accepted2024-11-07
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Date published2025-03-20
Laboratory studies of hydraulic fracturing of intersecting boreholes in a non-uniform stress field
This study focuses on the features of hydraulic fracture propagation in intersecting boreholes in polymethyl methacrylate blocks in a non-uniform stress field. Glycerol aqueous solution and plasticine were used as the working fluids. According to linear fracture mechanics, a stress concentrator at the borehole intersection contributes to the beginning of crack formation, with further crack propagation occurring in the plane containing their axes. The relevance of this study is due to the search for innovative approaches and the development of technological solutions to address the issue of effective longitudinal crack formation and its further propagation in a rock mass under unfavourable stress field conditions. This paper provides a scheme of laboratory stand operation and a general view of the sealing packers used to isolate a specified interval when performing tests. The graphs of glycerol pressure versus injection time are presented, and the breakdown pressure in the blocks is specified. The shape of fractures formed during the indentation of plasticine into the borehole system was investigated. The findings of physical modelling indicate that longitudinal cracks are predominantly formed in the boreholes. The deviation of the crack trajectory from the vertical plane containing the borehole axes is primarily affected by the magnitude of the horizontal compressive stress field rather than the increase in the angle between them. In addition, the angles of inclination of the longitudinal crack plane measured at its intersection with the side face of the block are specified.
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Date submitted2024-03-20
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Date accepted2024-11-07
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Date published2025-02-27
Analysis of the stress state of rocks transformation near a horizontal well during acid treatment based on numerical simulation
The article presents an overview of the assessment and modelling of the stress state of rocks in the near-wellbore zone of horizontal wells during acid stimulation of the formation for improving the efficiency of oil and gas field development. A numerical finite element model of near-wellbore zone of the reservoir drilled by a horizontal section was compiled using one of oil fields in the Perm Territory as an example. The distribution of physical and mechanical properties of the terrigenous reservoir near the well was determined considering transformation under the action of mud acid for different time periods of its injection. Multivariate numerical simulation was performed and the distribution of horizontal and vertical stresses in near-wellbore zone was determined with regard for different values of pressure drawdown and changes in stress-strain properties depending on the area of mud acid infiltration. It was found that a change in elastic modulus and Poisson's ratio under the influence of acid led to a decrease in stresses in near-wellbore zone. Analysis of the stress distribution field based on the Coulomb – Mohr criterion showed that the minimum safety factor of rock even after the effect of mud acid was 1.5; thus, under the considered conditions of horizontal well modelling, the reservoir rock remained stable, and no zones of rock destruction appeared.
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Date submitted2023-04-10
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Date accepted2024-11-07
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Date published2025-02-25
Consideration of the geomechanical state of a fractured porous reservoir in reservoir simulation modelling
This paper presents reservoir simulation modeling of a hydrocarbon accumulation with a fractured porous reservoir, incorporating the geomechanical effects of fracture closure during variations in formation pressure. The fracture permeability parameter is derived from the impact of stress on fracture walls. The fracturing parameter is determined based on 3D seismic data analysis. A permeability reduction model is implemented in the tNavigator reservoir simulation platform. The proposed approach improves the convergence of formation pressure dynamics in well data while maintaining flow rate and water cut adaptation accuracy. This results in enhanced formation pressure prediction and optimization of the pressure maintenance system.
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Date submitted2023-07-31
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Date accepted2024-11-07
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Date published2025-02-25
Environmental assessment of biochar application for remediation of oil-contaminated soils under various economic uses
- Authors:
- Tatiana V. Minnikova
- Sergey I. Kolesnikov
Remediation is an important area of oil-contaminated soil restoration in Russia, since oil refining industry is the major one for Russia and neighbouring countries, and the issues of environmentally effective and economically profitable remediation of oil contamination have not yet been solved. Soils under various economic uses have different surface areas and degrees of soil particles envelopment with oil due to the presence or absence of cultivation, the amount of precipitation and plant litter. The introduction of various substances for remediation into oil-contaminated soils of steppes (arable land), forests, and semi-deserts, considering their differences, gives different results. Biochar is coal obtained by pyrolysis at high temperatures and in the absence of oxygen. The uniqueness of this coal lies in the combination of biostimulating and adsorbing properties. The purpose of the study is to conduct an environmental assessment of biochar application for remediation of oil-contaminated soils under various economic uses. The article compares the environmental assessments of biochar application in oil-contaminated soils with different particle size fraction. The following indicators of soil bioactivity were determined: enzymes, indicators of initial growth and development intensity of radish, microbiological indicators. We found that the most informative bioindicator correlating with residual oil content is the total bacteria count, and the most sensitive ones are the roots length (ordinary chernozem and brown forest soil) and the shoots length (brown semi-desert soil). The use of biochar on arable land and in forest soil (ordinary chernozem and brown forest soil) is less environmentally efficient than in semi-desert soil (brown semi-desert soil). The study results can serve to develop measures and managerial and technical solutions for remediation of oil-contaminated soils under various economic uses.
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Date submitted2024-03-29
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Date accepted2024-11-07
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Date published2025-02-26
Well killing with absorption control
The development of new fields with low-permeability reservoirs required the introduction of new production technologies, of which the most significant for well killing and underground repair were multi-ton hydraulic fracturing, the simultaneous operation of two or three development sites by one well grid, and an increase in the rate of fluid extraction. These global decisions in field development have led to the need to search for new effective materials and technologies for well killing. The article is devoted to the analysis of problems associated with the process of killing production wells in fields characterized by increased fracturing, both natural and artificial (due to hydraulic fracturing), with reduced reservoir pressure and a high gas factor. The relevance of the analysis is due to the increase in the number of development sites where complications arise when wells are killed. Particular attention is paid to technical solutions aimed at preserving the filtration and capacity properties of the bottomhole formation zone, preventing the absorption of process fluid, and blocking the manifestation of gas. The classification of block-packs used in killing is given, based on the nature of the process fluid. Suspension thickened water-salt solutions are considered, forming a waterproof crust on the surface of the rock, which prevents the penetration of water and aqueous solutions into the formation. This approach ensures the safety and efficiency of killing operations, especially when working with formations in which maintaining water saturation and preventing the ingress of the water phase are of critical importance. Modern trends in the development of technology are revealed, and promising areas for further improvement of well killing with absorption control are outlined.
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Date submitted2021-12-20
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Date accepted2024-05-02
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Date published2024-08-26
A new formula for calculating the required thickness of the frozen wall based on the strength criterion
- Authors:
- Mikhail А. Semin
- Lev Yu. Levin
The study delves into the elastoplastic deformation of a frozen wall (FW) with an unrestricted advance height, initially articulated by S.S.Vyalov. It scrutinizes the stress and displacement fields within the FW induced by external loads across various boundary scenarios, notably focusing on the inception and propagation of a plastic deformation zone throughout the FW's thickness. This delineation of the plastic deformation zone aligns with the FW's state of equilibrium, for which S.S.Vyalov derived a formula for FW thickness based on the strength criterion. These findings serve as a pivotal launchpad for the shift from a one-dimensional (1D) to a two-dimensional (2D) exploration of FW system deformation with finite advance height. The numerical simulation of FW deformation employs FreeFEM++ software, adopting a 2D axisymmetric approach and exploring two design schemes with distinct boundary conditions at the FW cylinder's upper base. The initial scheme fixes both vertical and radial displacements at the upper base, while the latter applies a vertical load equivalent to the weight of overlying soil layers. Building upon the research outcomes, a refined version of S.S.Vyalov's formula emerges, integrating the Mohr – Coulomb strength criterion and introducing a novel parameter – the advance height. The study elucidates conditions across various soil layers wherein the ultimate advance height minimally impacts the calculated FW thickness. This enables the pragmatic utilization of S.S.Vyalov's classical formula for FW thickness computation, predicated on the strength criterion and assuming an unrestricted advance height.
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Date submitted2023-07-27
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Date accepted2024-06-03
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Date published2024-12-25
Normalized impulse response testing in underground constructions monitoring
Impulse Response testing is a widespread geophysical technique of monolithic plate-like structures (foundation slabs, tunnel lining, and supports for vertical, inclined and horizontal mine shafts, retaining walls) contact state and grouting quality evaluation. Novel approach to data processing based on normalized response attributes analysis is presented. It is proposed to use the energy of the normalized signal calculated in the time domain and the normalized spectrum area and the average-weighted frequency calculated in the frequency domain as informative parameters of the signal. The proposed technique allows users a rapid and robust evaluation of underground structure’s grouting or contact state quality. The advantage of this approach is the possibility of using geophysical equipment designed for low strain impact testing of piles length and integrity to collect data. Experimental study has been carried out on the application of the technique in examining a tunnel lining physical model with a known position of the loose contact area. As examples of the application of the methodology, the results of the several monolitic structures of operating municipal and transport infrastructure underground structures survey are presented. The applicability of the technique for examining the grouting of the tunnel lining and the control of injection under the foundation slabs is confirmed. For data interpretation the modified three-sigma criteria and the joint analysis of the attribute’s behavior were successfully used. The features of the field work methodology, data collection and analysis are discussed in detail. Approaches to the techniques' development and its application in the framework of underground constructions monitoring are outlined. The issues arising during acoustic examination of reinforced concrete plate-like structures are outlined.
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Date submitted2024-06-12
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Date accepted2024-07-18
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Date published2024-07-26
Development of parameters for an industry-specific methodology for calculating the electric energy storage system for gas industry facilities
- Authors:
- Ivan S. Tokarev
The issue of determining the main parameters of electric energy storage systems – power and energy intensity – is being considered, the determination of which is a fundamentally important task when introducing such devices into the power supply systems of enterprises for both technical (technological) and economic reasons. The work analyzes problems that can be solved by installing electricity storage systems at gas industry facilities. An industry-wide methodology has been developed for calculating the parameters of an electricity storage system based on traditional methods and methods aimed at minimizing the standardized cost of electricity with adaptation to the conditions of the gas industry. A distinctive feature of the presented methodology is the ability to determine the power and energy intensity of electricity storage systems when performing several functions. The methodology was tested at a typical gas industry facility – the Yarynskaya compressor station of OOO Gazprom Transgaz Ukhta, a characteristic feature of which is an autonomous power supply system. An example is given of calculating the electricity storage normalized cost using an improved LCOS indicator, which takes into account the effect of changing the fill factor of the electrical load schedule on the amount of gas consumption by a power plant for its own needs. To confirm the economic efficiency of introducing electricity storage systems calculated using the above methodology, calculations of the integral effect, net present value and efficiency index are presented.
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Date submitted2023-03-14
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Date accepted2023-10-25
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Date published2024-04-25
Predictive assessment of ore dilution in mining thin steeply dipping deposits by a system of sublevel drifts
The purpose of research is the study of stress-strain state of marginal rock mass around the stope and predictive assessment of ore dilution with regard for changes in ore body thickness in mining thin ore deposits on the example of the Zholymbet mine. Study of the specific features of the stress-strain state development was accomplished applying the methodology based on numerical research methods taking into account the geological strength index (GSI) which allows considering the structural features of rocks, fracturing, lithology, water content and other strength indicators, due to which there is a correct transition from the rock sample strength to the rock mass strength. The results of numerical analysis of the stress-strain state of the marginal part of the rock mass using the finite element method after the Hoek – Brown strength criterion made it possible to assess the geomechanical state in the marginal mass provided there are changes in ore body thickness and to predict the volume of ore dilution. It was ascertained that when mining thin ore deposits, the predicted value of ore dilution is influenced by the ore body thickness and the GSI. The dependence of changes in ore dilution values on the GSI was recorded taking into account changes in ore body thickness from 1 to 3 m. Analysis of the research results showed that the predicted dimensions of rock failure zone around the stopes are quite large, due to which the indicators of the estimated ore dilution are not attained. There is a need to reduce the seismic impact of the blasting force on the marginal rock mass and update the blasting chart.
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Date submitted2022-11-29
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Date accepted2023-03-02
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Date published2023-10-27
New data on the composition of growth medium of fibrous diamonds from the placers of the Western Urals
This article presents the results of studying microinclusions of fluids/melts in diamonds from the placers of the Krasnovishersky District (western slope of the Middle/Northern Urals), which make it possible to establish the evolution of diamond-forming media in the subcontinental lithospheric mantle of the eastern margin of the East European craton. Impurity composition of the studied crystals reveals three different types of diamonds, the formation of which was associated with separated metasomatic events. Microinclusions in B-type diamonds containing A and B nitrogen defects reflect an older metasomatic stage characterized by the leading role of silicic and low-Mg carbonatitic fluids/melts. The second stage is associated with the growth of A-type diamonds containing nitrogen exclusively in the form of A-centers. At this stage, the formation of diamonds was related with low-Mg carbonatitic media, more enriched in MgO, CaO, CO2, and Na2O compared to B-type diamonds. The third stage probably preceded the eruption of the transporting mantle melt and led to the formation of C-type diamond containing A and C nitrogen defect centers and microinclusions of silicic to low-Mg carbonatitic composition. The recorded trend in the evolution of diamond-forming fluids/melts is directed towards more carbonatitic compositions. Fluids/melts are probably sourced from eclogitic and pyroxenitic mantle substrates.
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Date submitted2022-08-24
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Date accepted2023-02-15
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Date published2023-08-28
Modelling of the stress-strain state of block rock mass of ore deposits during development by caving mining systems
The article is devoted to the analysis of approaches to modeling the stress-strain state of a block rock mass in the vicinity of a single mine workings and in the area of rock cantilever influence during the development of the Khibiny apatite-nepheline deposits. The analysis of the existing in international engineering practice ideas about tectonic disturbances as a geomechanical element and the experience of predicting the stress-strain state of a block rock mass was carried out. On the basis of the analysis, the formulation of the basic modeling tasks is carried out and its main results are presented. Methodological recommendations for solving similar problems were developed.
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Date submitted2022-04-03
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Date accepted2023-03-02
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Date published2023-12-25
Specifics of geotechnical risk control in the design of underground structures
The underground space development is associated with the emergence of complex and dangerous situations, often leading to accidents. The condition for their development is the potential geotechnical risks. High-quality execution and analysis of design work at all the stages of design, starting from the early stages, is one of the effective ways to control risks. Clarification of the characteristics and features of the rock mass adjacent to the projected underground structure makes it possible to identify the potential cause of the occurrence of an adverse event with a certain probability during the construction and operation of an underground structure. The purpose of a qualitative risk analysis is to identify risk factors in underground construction. The value of the total geotechnical risk, expressed by the sum of each of the possible risks, should be numerically estimated at the design stage of a specific underground facility. At the same time, it is extremely important to develop a methodology for managing geotechnical risks, which would make it possible to assess their probability of development at an early stage of project preparation and propose measures to reduce or prevent them. This technique is given in the article. The results of the study conducted in accordance with the presented methodology showed that geotechnical risk control proved an effective method in preventing accidents during underground construction.
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Date submitted2021-10-31
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Date accepted2023-03-02
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Date published2023-12-25
Improvement of technological schemes of mining of coal seams prone to spontaneous combustion and rock bumps
On the example of the Alardinskaya mine, the problem of underground mining of seams prone to spontaneous combustion and rock bumps in the conditions of the Kondomsky geological and economic region of the Kuznetsk coal basin is considered. The contradictions in the requirements of regulatory documents for the width of the inter-panel coal pillars in the mining of seams with longwalls in conditions of endogenous fire hazard and in the mining of seams that are dangerous due to geodynamical phenomena are discussed. These contradictions impede the safe mining of seams using traditionally used layouts with the danger of spontaneous combustion of coal and rock bumps. A mining-geomechanical model is presented, which is used for numerical three-dimensional simulation of the stress-strain state of a rock mass with various layouts for longwall panels using the finite element method. The results of the numerical analysis of the stress state of the rock mass immediately before the rock bump are presented, and the main factors that contributed to its occurrence during the mining of the seam are established. A dangerous degree of stress concentration in the coal seam near the leading diagonal entries is shown, especially in conditions of application of abutment pressure from the edge of panels’ gob. The analysis of the features of stress distribution in the inter-panel pillar at different widths is carried out. Recommendations for improving the layout for the development and mining of coal seams that are prone to spontaneous combustion and dangerous in terms of rock bumps in the conditions of Alardiskaya mine have been developed. The need for further studies of the influence of pillars for various purposes, formed during the mining of adjacent seams, on the stress-strain state of previously overmined and undermined seams is shown.
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Date submitted2022-06-20
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Date accepted2023-01-10
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Date published2023-08-28
Laboratory, numerical and field assessment of the effectiveness of cyclic geomechanical treatment on a tournaisian carbonate reservoir
Results are discussed for evaluation of effectiveness of the cyclic geomechanical treatment (CGT) on a Tournaisian carbonate reservoir. Analysis of laboratory experiments performed according to a special program to assess permeability changes for Tournaisian samples under cyclic changes in pore pressure is presented. The main conclusion is the positive selectivity of the CGT: an increase in permeability is observed for samples saturated with hydrocarbons (kerosene) with connate water, and maximal effect is related to the tightest samples. For water-saturated samples, the permeability decreases after the CGT. Thus, the CGT improves the drainage conditions for tight oil-saturated intervals. It is also confirmed that the CGT reduces the fracturing pressure in carbonate reservoirs. Using flow simulations on detailed sector models taking into account the results of laboratory experiments, a possible increase in well productivity index after CGT with different amplitudes of pressure variation was estimated. Results of a pilot CGT study on a well operating a Tournaisian carbonate reservoir are presented, including the interpretation of production logging and well testing. The increase in the well productivity index is estimated at 44-49 % for liquid and at 21-26 % for oil, with a more uniform inflow profile after the treatment. The results of the field experiment confirm the conclusions about the mechanisms and features of the CGT obtained from laboratory studies and flow simulations.
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Date submitted2022-10-26
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Date accepted2023-02-13
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Date published2023-07-19
Determination of the grid impedance in power consumption modes with harmonics
The paper investigates the harmonic impedance determination of the power supply system of a mining enterprise. This parameter is important when calculating modes with voltage distortions, since the determined parameters of harmonic currents and voltages significantly depend on its value, which allow the most accurate modeling of processes in the presence of distortions in voltage and current. The power supply system of subsurface mining is considered, which is characterized by a significant branching of the electrical network and the presence of powerful nonlinear loads leading to a decrease in the power quality at a production site. The modernization of the mining process, the integration of automated electrical drive systems, renewable energy sources, energy-saving technologies lead to an increase in the energy efficiency of production, but also to a decrease in the power quality, in particular, to an increase in the level of voltage harmonics. The problem of determining the grid harmonic impedance is solved in order to improve the quality of design and operation of power supply systems for mining enterprises, taking into account the peculiarities of their workload in the extraction of solid minerals by underground method. The paper considers the possibility of determining the grid impedance based on the measurement of non-characteristic harmonics generated by a special nonlinear load. A thyristor power controller based on phase regulation of the output voltage is considered as such a load. Simulation computer modeling and experimental studies on a laboratory test bench are used to confirm the proposed method. The recommendations for selecting load parameters and measuring device connection nodes have been developed.
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Date submitted2022-01-21
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Date accepted2022-11-14
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Date published2023-08-28
Strategy of mine ventilation control in optimal mode using fuzzy logic controllers
- Authors:
- Aleksei V. Kashnikov
- Yuri V. Kruglov
The issues related to improving the efficiency of automatic ventilation control systems of mines that regulate the air supply to the mine in accordance with the need are considered. During the tests of such a system in the 3RU mine of OAO Belaruskali, the shortcomings of its existing, implementation, associated with the incorrect choice of the most difficult-to-ventilate direction, were revealed. The possibilities of implementing a control strategy, in which the system automatically determines the optimal configuration of the operating modes of fans and regulators, are demonstrated. As an alternative to the implemented algorithms, it is proposed to use a fuzzy control device to account for the nonlinearity of the dependence of the input and output parameters of ventilation equipment and to set the conditions for the optimal operating mode of the system in a declarative form. To assess the effectiveness of the proposed approach, the data of simulation modeling of the current ventilation mode and the transition from one ventilation mode to another are analyzed with comparison with the actual data of the system operation. The simulation results show that the use of an upgraded control scheme for the main ventilation fan based on fuzzy logic in the implementation of automatic ventilation control systems makes it possible to eliminate the possibility of a shortage of fresh air in the regulated directions of its movement, as well as excessive power consumption of the main ventilation fan.
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Date submitted2022-07-15
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Date accepted2022-12-13
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Date published2023-02-27
Assessment of the efficiency of occupational safety culture management in fuel and energy companies
The results of development, testing and implementation of the process of occupational safety culture management in a fuel and energy company including the assessment of current state, assessment of deviation, formation of control action and its implementation are presented. Using the methods of mathematical analysis, the components of occupational safety culture and criteria for their evaluation were developed. As a control action, a procedure for conducting behavioural safety audit was elaborated and implemented. Proceeding from the results of analysing average ratings of safety culture components among the employees prior to and after the introduction of behavioural safety audit, it was concluded that there was a statistically significant increase in the average values of 12 out of 16 ratings of safety culture components. Analysis of the results of 1,011 audits showed the absence of an “alarm area” at the enterprise. Introduction of the developed process management model promotes an increase in the efficiency of attaining a high level of occupational safety culture in fuel and energy companies.
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Date submitted2022-07-15
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Date accepted2022-12-13
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Date published2023-02-27
Mathematical modelling of displacement during the potash ores mining by longwall faces
In favourable mining conditions, in particular at the Starobinskoye potash deposit (Belarus), longwall mining systems are used. They cause a high human-induced load on the subsoil, including intense deformation of the ground surface. The presented investigations are aimed at studying the dynamics of the ground surface displacement during the longwall face advance. Mathematical modelling was carried out in an elastic-plastic formulation with numerical implementation by the finite element method. The condition for the roof rocks collapse was opening of the contact between the seams when its boundaries were reached by shear fractures or formation of the tensile stresses area at the outcrop. With the working front advance, an increase in subsidence is observed, followed by its stabilization to a value determined by the process parameters of mining operations and the physical and mechanical properties of collapsed rocks. In this case, each point of the ground surface experiences sign-alternating horizontal deformations: when the front approaches, it causes tension, and when it moves away, compression. The obtained results of mathematical modelling are in good agreement with the data of instrumental measurements of the ground surface displacements, which indicates the adequate description of the rock mass deformation during the slice excavation of sylvinite seams by longwall faces.
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Date submitted2022-11-08
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Date accepted2022-11-21
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Date published2023-02-27
Assessment of the role of the state in the management of mineral resources
Mineral resources as natural capital can be transformed into human, social and physical capital that guarantees the sustainable development of a country, exclusively through professional public management. Public management of a country's mineral resource potential is seen as an element of transnational governance which provides for the use of laws, rules and regulations within the jurisdictional and sectoral capabilities of the state, minimising its involvement as a producer of minerals. The features of the ideology of economic liberalism, which polarises the societies of mineral-producing countries and denies the role of the state as a market participant, have been studied. The analysis of the influence of the radical new order of neoliberal world ideology on the development of the extractive sector and state regulation has been presented.
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Date submitted2022-09-30
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Date accepted2022-11-28
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Date published2022-12-29
Intelligent monitoring of the condition of hydrocarbon pipeline transport facilities using neural network technologies
The national strategic goal of the Russian Federation is to ensure the safety of critical technologies and sectors, which are important for the development of the country's oil and gas industry. The article deals with development of national technology for intelligent monitoring of the condition of industrial facilities for transport and storage of oil and gas. The concept of modern monitoring and safety control system is developed focusing on a comprehensive engineering control using integrated automated control systems to ensure the intelligent methodological support for import-substituting technologies. A set of approved algorithms for monitoring and control of the processes and condition of engineering systems is proposed using modular control robotic complexes. Original intelligent models were developed for safety monitoring and classification of technogenic events and conditions. As an example, algorithms for monitoring the intelligent safety criterion for the facilities and processes of pipeline transport of hydrocarbons are presented. The research considers the requirements of federal laws and the needs of the industry.
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Date submitted2022-05-18
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Date accepted2022-07-21
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Date published2022-11-10
Improving the method for assessment of bending stresses in the wall of an underground pipeline
- Authors:
- Ruslan V. Aginey
- Alexei A. Firstov
Brief information about modern methods for determining the bending stresses of the extended sections of underground main pipelines without access to the pipeline generatrix is given. The necessity of modernizing methods based on determining the configuration of the pipeline axis from the soil surface with subsequent calculation of bending stresses based on the obtained data is substantiated. A mathematical model that allows to calculate the optimal parameters for surveying the axis of the pipeline from the soil surface for a pipeline of arbitrary configuration and depth, when planning a study, is proposed. Bench tests of the BITA-1 pipeline finder were carried out to determine the error in measuring the depth of the pipeline axis. It is proved that the deviations of the pipeline finder data relative to the true values in narrow depth intervals follow a normal distribution and do not change their sign. The confidence intervals of the error in determining the depth of the pipeline axis for the BITA-1 device are presented.
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Date submitted2021-03-31
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Date accepted2022-04-26
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Date published2022-11-03
Features of obtaining metallurgical products in the solid-state hydride synthesis conditions
- Authors:
- Andrey G. Syrkov
- Lyudmila A. Yachmenova
A scientific substantiation of solid-phase feedstock choice and preparation has been carried out, and the thermodynamic and kinetic aspects of solid-state hydride synthesis (SHS) of metal products have been analyzed using the nickel dichloride reduction as an example. The preliminary dehydration modes and methods for controlling the complete removal of crystalline water from chloride raw materials and Olenegorsk superconcentrate, which is natural oxide raw material, are described. Conditions, including initial solid chloride particle sizes, are established under which diffusion complications of reduction to metal in methyldichlorosilane vapor are minimized. Thermodynamic estimates of nickel chlorides and oxides reduction possibility, iron and copper with ammonia and methane at temperatures of 400-1000 K in equilibrium conditions have been carried out. It has been shown that the stoichiometric coefficients of the nickel dichloride in ammonia overall reduction reaction calculated by thermodynamic modeling are in agreement with experimental data. In contrast to the copper dichloride reduction, for nickel dichloride the formation of metal monochloride at the intermediate stage is uncharacteristic, which is associated with a higher thermal stability of nickel dichloride. The main kinetic regularities of the reduction of nickel, copper, and iron to metal under SHS conditions in ammonia, monosilane, and methane, as well as the nickel dichloride with methyldichlorosilane vapor and methane successive reduction, are considered. Approximation of experimental data by topochemical equations in a linear form showed that for reduction degrees a up to 0.7-0.8, these data are satisfactorily described by the Roginsky – Schultz equation. For a > 0,8 the “shrinking sphere” model works better, which confirms the localization of the solid-state reduction reaction at the interface, moves deep into the crystal with the formation of a of interlocked metal germs. The importance and prospects of the results obtained for the theory development of metallurgical processes, deep complex processing of natural iron oxide raw materials, metal products and new generation materials production, including superhydrophobic ones, are discussed. The relevance of the study from the point of view of applying the method of physical and chemical analysis to the study of complex heterogeneous metallurgical processes is noted.
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Date submitted2021-11-17
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Date accepted2022-04-06
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Date published2022-11-10
Method for predicting the stress state of the lining of underground structures of quasi-rectangular and arched forms
- Authors:
- Maksim A. Karasev
- Tien Tai Nguyen
A method for predicting the stress-strain state of the lining of underground structures, the shape of the cross-section of which is different from the circular outline, is considered. The main task of the study is to develop a methodology for assessing the influence of the parameters of the cross-section shape of underground structures on the stress state of the lining. To solve this problem, a method for calculating the stress state of the lining for arched tunnels with a reverse arch and quasi-rectangular forms is substantiated and developed. The methodology was tested, which showed that the accuracy of the prediction of the stress state of the lining is sufficient to perform practical calculations. An algorithm for multivariate analysis of the influence of the cross-sectional shape of underground structures of arched and quasi-rectangular shapes on the stress state of the lining is proposed. Parametric calculations were performed using the developed algorithm and regularities of the formation of the stress state of the lining of underground structures for various engineering and geological conditions, as well as the initial stress state field, were obtained. A quantitative assessment of the influence of geometric parameters of tunnels on their stress-strain state was performed.
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Date submitted2022-04-18
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Date accepted2022-06-15
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Date published2022-07-26
Results and prospects of geological mapping of the Arctic shelf of Russia
- Authors:
- Evgeny A. Gusev
The results of compiling the sets of the State Geological Map at a scale of 1:1,000,000 for the Arctic continental shelf of Russia are analyzed. Results are summed up, and the main problems of geological mapping are outlined. The results of geological and geophysical studies of the Arctic Ocean are of great importance for deciphering the geological evolution. The Arctic shelf is the widest shelf in the world, while the spreading ocean basin is one of the narrowest and is characterized by anomalous structural features. The main problems of geological mapping include identification the sedimentary cover/folded basement boundary, interpretation the geodynamic evolution of the shelf and adjacent ocean, determining the rates of sedimentation and stratigraphic subdivision of the sedimentary cover due to a small number of key boreholes. It is promising to further study problem areas with unclear features of geological structure as well as small-scale mapping in areas of industrial development on the Arctic continental shelf.
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Date submitted2021-10-31
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Date accepted2022-04-26
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Date published2022-07-13
Identification of structural control factors of primary gold ore occurrences by method of unmanned aeromagnetic survey by the example of the Neryungrisky district of Yakutia
The long-term development of the geophysical industry, in which the methods of magnetometry are in maximum demand, as the simplest in instrumental and methodological execution, has determined the development of remote measurement methods implemented both from space and airborne carriers. The necessity to use the latter as an obligatory component of field surveys, providing coverage of significant areas, determines the need for using the unmanned low-tonnage carriers. Their use is implemented to search for predictive elements of structural (spatial, genetic) control of endogenous gold ore occurrences that allow predictive constructions, i.e., solving the problem of increasing gold reserves, which is being performed within the framework of federal programs. The purpose of the survey is to develop a system of instrumental and subsequent interpretation approaches in the organization of unmanned magnetometer survey, implemented for structural and geological mapping by the example of the Neryungrinsky district of Yakutia. Within the framework of the digital model formation of the relief and the anomalous magnetic field, a survey method using an unmanned aircraft, its technical characteristics are considered; the analysis and the author's modification of the office analysis of magnetometry data are performed. Based on the obtained materials, a physical and geological model of the investigated area was created, which is presented in the form of a geological and structural cut, accompanied by the physical characteristics of the structural and material complexes. The refinement of the physical and geological model was implemented by a joint morphostructural analysis of the remote base and the anomalous magnetic field using the results of quantative interpretation of the anomalous magnetic field. The result of the study is presented by an updated geological basis with the allocation of promising ore sites for their detailing as part of the planned large-scale geological and geophysical surveys. The scientific novelty of the work consists in the synthesis of the tried and tested methods of unmanned aeromagnetometric measurements and geostructural reconstructions, which allow the processing of both potential and non-potential geofields.