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apatite flotation

Geotechnical Engineering and Engineering Geology
  • Date submitted
    2024-05-03
  • Date accepted
    2024-07-11
  • Date published
    2025-04-02

Assessment of ancylite ore dressability by flotation method

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For more than 50 years, most rare earth elements were extracted from carbonatite deposits, which can contain different rare earth phases, but the main extracted minerals are bastnaesite, monazite and xenotime. Many studies focused on the improvement and development of dressing circuits for ores of these minerals. However, in some carbonatite complexes, rare earth deposits are composed partly or mainly of ancylite ores. This type of rare earth ores was very poorly studied in terms of dressability – previous experiments with ancylite ores are rare and not productive enough. Ancylite is the main concentrator of rare earth elements in most carbonatite complexes of the Devonian Kola Alkaline Province (northwest Russia). Dressability of ancylite ore from the Petyayan-Vara carbonatite field in the Vuorijärvi alkaline-ultramafic complex was assessed using the flotation method. The complex is one of the most potential rare earth deposits associated with carbonatites in the Kola Region. Petrographic and mineralogical studies demonstrated the occurrence of abundant iron and barite oxide inclusions in ancylite, which imposes restrictions on physical separation of these three minerals. The study of petrogeochemical and mineralogical composition of fractions formed during mechanical grinding of ores to a size less than 2.0 mm showed that even at this stage of sample preparation, the finest-grained fractions (less than 0.071 mm) were enriched in ancylite (to 19 vol.% or more with a content of 15 vol.% in ore). Three classes of reagents were considered as collectors in flotation experiments: fatty acids, alkyl hydroxamic acids, and amino acid derivatives. The reagent from the amino acid derivative class was highly efficient. The use of such a collector in combination with sodium hexametaphosphate depressant made it possible to obtain a flotation concentrate in an open circuit with total rare earth oxides content 33.4 wt.% at 64.7 % extraction.

How to cite: Mitrofanova G.V., Kozlov E.N., Fomina E.N., Chernousenko E.V., Chernyavskii A.V., Dorozhanova N.O. Assessment of ancylite ore dressability by flotation method // Journal of Mining Institute. 2025. p. EDN UOHOQP
Geotechnical Engineering and Engineering Geology
  • Date submitted
    2024-04-24
  • Date accepted
    2024-09-24
  • Date published
    2024-11-12

Study and justification of the combination of beneficiation processes for obtaining flake graphite from technogenic carbon-containing dusts

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The most important task of modern production development is to provide the mineral and raw materials sector of the economy with resources included in the list of strategic raw materials, including flake graphite. In addition to natural raw materials, the source of its obtaining can be metallurgical production wastes not involved in processing. Development of metallurgical dust beneficiation technology will solve the problem of obtaining high-purity flake graphite with a crystal structure close to ideal and in demand in the production of high-tech materials. It will allow creating a renewable raw material base of graphite and utilising metallurgical production wastes. The research included the study of dust beneficiation by coarseness, magnetic and flotation methods, the influence of dust disintegration processes on beneficiation indicators. Based on the established technological properties of the components of dusts, magnetic, flotation and gravity beneficiation methods can be applied for their separation in different sequence. It is shown that dusts from different sites have different enrichability by these methods, and it should be taken into account when developing a complex technology of their processing. The degree of beneficiation increases in a row of dusts from the blast furnace shop (BF) – electric steel smelting shop (ESS) – oxygen-converter shop (OCS). The method of grinding has a significant influence on the separation indicators – at dry grinding in a centrifugal-impact mill with subsequent pneumatic classification the quality of graphite concentrates increases by 22.7 % of carbon for BF dust and by 13.48 % of carbon for ESS dust. OCS dust beneficiation indicators are high at coarse grinding with steel medium – mass fraction of carbon 96.1 %.

How to cite: Orekhova N.N., Fadeeva N.V., Musatkina E.N. Study and justification of the combination of beneficiation processes for obtaining flake graphite from technogenic carbon-containing dusts // Journal of Mining Institute. 2024. Vol. 269. p. 777-788. EDN UNUYXS
Geotechnical Engineering and Engineering Geology
  • Date submitted
    2024-04-12
  • Date accepted
    2024-09-05
  • Date published
    2024-11-12

Promising reagents for the extraction of strategic metals from difficult-to-enrich mineral raw materials

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The need of the mining and processing industry for new types of directional reagents is due to the deterioration of the material composition of the processed ores. Low Au content (less than 0.5-1.0 g/t), finely dispersed Au inclusions (0.1-10.0 microns) in the ore, similar properties of the separated minerals have an extremely negative effect on flotation performance when using traditional reagents, which leads to significant losses of valuable metal with enrichment tailings. Expanding the range of domestic flotation reagents based on the latest achievements of fundamental research and their targeted application at mining and processing companies will compensate for the negative impact of the mineral composition of raw materials and ensure maximum extraction of strategic metals from difficult-to-enrich ores. The use of modern research methods (scanning electron and laser microscopy, UV spectrophotometry, XRF and chemical analysis) made it possible to visualize the adsorption layer of new reagents-collectors of a number of dithiocarbamates with different structures of a hydrocarbon radical and an organic modifier on the surface of gold-containing sulfides. The amount of adsorbed reagents on the surface of minerals has been experimentally determined. The specific features of the fixation of reagents on minerals of various compositions led to optimal correlations of their consumption in the flotation process. Scientifically based reagent regimes ensured an increase in the gold content in the concentrate and a decrease in the loss of gold with tailings by 5-6 % during flotation enrichment of the refractory ore of the Malinovskoe deposit.

How to cite: Matveeva T.N., Gromova N.K., Lantsova L.B. Promising reagents for the extraction of strategic metals from difficult-to-enrich mineral raw materials // Journal of Mining Institute. 2024. Vol. 269. p. 757-764. EDN XAAEGH
Geotechnical Engineering and Engineering Geology
  • Date submitted
    2023-09-08
  • Date accepted
    2024-06-03
  • Date published
    2024-12-25

Modern approaches to barium ore benefication

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Barite is one of the critically important minerals in several industries, including the fuel and energy, nuclear, and medical sectors. For decades, its extraction did not require any complex techniques; however, with the depletion of rich barite-bearing veins around the world, the circumstances have changed. While the demand for barite is growing widely, it is necessary to optimize and improve the existing methods for benefication of barite and barite-containing ores, and create new approaches to extracting this mineral, as well as develop technogenic barite deposits accumulated in large quantities during the previous ore production. Dumps and tailings often demonstrate high barite content, while new mining technologies make its extraction cost-efficient. Russian and foreign papers of the last 14 years provide data on the current state of primary and technogenic deposits, areas of barite use and the approaches employed for its benefication. Considering the expansion of the range of barite applications, the growing need for the mineral in the oil and gas industry and the difficulties in developing new barite deposits in Russia, the importance of new approaches to the enrichment of ore tailings in polymetallic deposits is revealed.

How to cite: Yurkevich N.V., Grosheva T.V., Edelev A.V., Gureev V.N., Mazov N.A. Modern approaches to barium ore benefication // Journal of Mining Institute. 2024. Vol. 270. p. 977-993. EDN RZNPBK
Geotechnical Engineering and Engineering Geology
  • Date submitted
    2023-06-21
  • Date accepted
    2023-10-25
  • Date published
    2024-08-26

Specific action of collector from phosphoric acid alkyl esters class in flotation of apatite-nepheline ores

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Increasing amount of apatite-nepheline ores with complex mineral composition involved in processing, growing content of the associated minerals in ore which are similar in their floatability to apatite lead to the necessity of using highly selective collectors. Non-frothing flotation method gave a comparative assessment of floatability of pure minerals and demonstrated a high selectivity of the action of phosphoric acid esters in relation to apatite. The effect of four reagent modes differing in the number of selective synthetic collectors was studied using the example of flotation of an apatite-nepheline ore sample containing 17.27 % apatite and 40.18 % nepheline. Mineralogical analysis of crushed ore showed that it contained two apatite varieties – coarse-grained free and finer poikilitic as inclusions in rock-forming minerals. Free apatite opens and occurs as open grains even in coarse-grained (+0.16 mm) grades. Poikilitic apatite occurs as intergrowths with different minerals, mainly with nepheline and its alteration products (natrolite, spreustein, sodalite, etc.), and pyroxene. Optical microscopy demonstrated that a growing share of reagent from the phosphoric acid oxyethylated esters class in the composition of the collector mixture allows improving the quality of the produced apatite concentrates by reducing the number of apatite intergrowths with nepheline and pyroxenes in the concentrates. In the concentrate obtained in the most selective reagent mode, the intergrowths are characterized by a 50/50 and higher ratio in favour of apatite. Concentrates of lower quality comprised intergrowths with lower apatite content, to 20/80 or less.

How to cite: Mitrofanova G.V., Chernousenko E.V., Kompanchenko A.A., Kalugin A.I. Specific action of collector from phosphoric acid alkyl esters class in flotation of apatite-nepheline ores // Journal of Mining Institute. 2024. Vol. 268. p. 637-645. EDN CSNOBO
Geotechnical Engineering and Engineering Geology
  • Date submitted
    2022-05-17
  • Date accepted
    2023-04-03
  • Date published
    2024-02-29

Improvement of concentrate quality in flotation of low-rank coal

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Percentage of high-rank coal with low content of ash, moisture, and sulfur in total coal production output is low. Most of the produced coal has a low quality (lignite, bituminous coal: long-flame and fiery). Under increasing requirements for ecological cleanness of coal, the efficient use of coal products is only possible after improvement of their processing properties. The authors discuss the enhancement of flotation efficiency of low-rank coal using the mechanism of physisorption of a collecting agent in particle – bubble attachment. It is explained why the yield of concentrate with low ash content increases as a result of combination of collectors having different physical properties. It is shown that the surface activity of a heteropolar agent relative to the gas – liquid interface and the adsorption density of the agent govern its collecting properties. Based on the recovery – surface activity relationship, the correlation is found between the collecting activity of a chemical compound and the structure of its molecules. The combination of the collectors with different surface activity enables adjusting collectability and selectivity of the blend. The physisorption mechanism of collectors can be a framework for developing recommendations on modification of concentrate yield and ash content, and on selection of optimized ratios of surface activities of miscible collectors relative to the gas – liquid interface.

How to cite: Kondratev S.A., Khamzina T.A. Improvement of concentrate quality in flotation of low-rank coal // Journal of Mining Institute. 2024. Vol. 265. p. 65-77. EDN RJTNNI
Geotechnical Engineering and Engineering Geology
  • Date submitted
    2022-10-31
  • Date accepted
    2023-04-21
  • Date published
    2024-02-29

Study of the properties and action of polyelectrolytes in the treatment of the dressing plant’s discharges

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The organization of intrafactory water circulation at mining and processing enterprises, when production wastes and discharges are not sent to an external tailings dump, is an urgent environmental and economic task. Returning even a part of water into the technological process after preliminary treatment will significantly reduce the volume of polluted water discharged into tailings, which will reduce energy costs for waste transportation and the negative environmental impact. One of the wastes sent to the tailings during the ore dressing wastes from the Kovdor deposit to the tailings dump is the discharge of thickeners for the preparation of apatite flotation feed. In order to choose the effective discharge cleaning regime, the authors have evaluated the action of polyacrylamide flocculants. It has been discovered that the apatite and calcite particles interact more effectively with the anionic flocculant. This fact determines its advantage for the treatment of suspended particles. The influence of the residual concentration of a flocculant on the apatite flotation, where a part of the returned treated water goes, has been assessed. Compared to flotation with recycled water, there is a decrease of P2O5 extraction into apatite concentrate of equal quality. In order to obtain the required enrichment indicators on the treated water, it is necessary to adjust the collector (tall oil fatty acids) and depressor (liquid glass) costs.

How to cite: Mitrofanova G.V., Chernousenko E.V., Artemev A.V., Pospelova Y.P., Smirnova N.A., Barmin I.S. Study of the properties and action of polyelectrolytes in the treatment of the dressing plant’s discharges // Journal of Mining Institute. 2024. Vol. 265. p. 95-103. EDN CVUHNQ
Metallurgy and concentration
  • Date submitted
    2022-05-10
  • Date accepted
    2022-09-06
  • Date published
    2022-11-03

Flotation separation of titanite concentrate from apatite-nepheline-titanite ores of anomalous zones of the Khibiny deposits

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Titanium raw materials are widely used for the synthesis of various functional materials – sorbents of radionuclides and rare earth elements, various additives, filler pigments, etc. Since most of titanium concentrates are imported, in line with the import substitution program, production of titanite concentrate from apatite-nepheline ores of the Khibiny deposits is a promising trend for supplying national industry with titanium raw materials. The article presents the results of laboratory studies of flotation separation of titanite concentrate from apatite-nepheline-titanite ores extracted from the upper ore horizon of the Koashvinskoye deposit, where titanite-enriched ores are concentrated. Recovery of titanite concentrate was accomplished using two reagent modes – a mixture of alkyl hydroxamic and carboxylic acids with the addition of distilled tall oil and a mixture of tall oils with the addition of polyalkyl benzene sulfonic acids. The results of the research showed that the first flotation mode, which allows a selective recovery of titanite into the concentrate (titanite content in the concentrate was 93.5 %) is the most efficient. It was shown that flotation separation of titanite concentrate is preferable compared to the chemical method based on sulfuric acid leaching.

How to cite: Mitrofanova G.V., Marchevskaya V.V., Taran A.E. Flotation separation of titanite concentrate from apatite-nepheline-titanite ores of anomalous zones of the Khibiny deposits // Journal of Mining Institute. 2022. Vol. 256. p. 560-566. DOI: 10.31897/PMI.2022.81
Metallurgy and concentration
  • Date submitted
    2022-03-17
  • Date accepted
    2022-06-20
  • Date published
    2022-11-03

Assessment of collecting activity of physically sorbed reagents on the example of easily floatable coking coal sludge

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The article presents one of the new approaches to theoretical assessment of collecting ability of reagents. The efficiency of reagents-collectors with different chemical composition used for flotation of coking coals was studied. A comparative assessment of the flotation activity of kerosene, mineral oil, thermal gas oil, KETGOL and FLOTEK is given. The criteria of collecting activity of the above reagents-collectors for coal sludge flotation were specified. A correlation was established between the indicators of coal sludge flotation by the above reagents and their physical parameters. It is shown that the rate of spreading over water surface can characterize the flotation activity of reagents. Based on dependence of the collecting activity of a reagent on its rate of spreading along the “gas – liquid” interface and surface pressure, the main approaches to determining the structure and composition of molecules of an effective flotation collector can be determined. A new concept of the function performed by a physically sorbed collector in the elementary act of flotation and a criterion for the flotation activity of reagents used in coal sludge beneficiation are proposed. It is shown that the collector used in coal flotation, in addition to hydrophobizing the surface of the extracted particles, should reduce the induction time and remove the kinetic constraint on formation of a flotation aggregate.

How to cite: Kondratev S.A., Khamzina T.A. Assessment of collecting activity of physically sorbed reagents on the example of easily floatable coking coal sludge // Journal of Mining Institute. 2022. Vol. 256. p. 549-559. DOI: 10.31897/PMI.2022.52
Metallurgy and concentration
  • Date submitted
    2022-05-03
  • Date accepted
    2022-07-21
  • Date published
    2022-11-03

Determination of rational steam consumption in steam-air mixture flotation of apatite-nepheline ores

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Relevance of the study is determined by the decisions taken to increase the production volume of certain commercial products from mineral raw materials. The scale, impact and consequences of the projects on developing the resource-saving technologies for beneficiation of mineral raw materials are socially significant, and the economic growth of mining production complies with the sustainable development goals. The aim of the study is to develop the flotation circuit and mode that improve the technological performance of beneficiation of apatite-nepheline ores of the Khibiny Massif in the Kola Peninsula. The scientific idea of ​​the work is to develop the flotation circuit, the movement of beneficiation products in which ensures a major increase in the content of the recovered component in the rougher flotation procedure with a simultaneous increase in dressability of the material. The above condition is met when mixing the feedstock with rough concentrate. Recovery of the valuable component from the resulting mixture is accomplished in a mode differing from the known ones in that the heat of steam condensation is used to increase water temperature in the interphase film between the particle and the bubble. For pulp aeration during flotation, a mixture of air and hot steam is used as the gas phase. A high recovery of the valuable component in ore flotation according to the developed circuit and mode is facilitated by increasing water temperature in wetting films due to the steam condensation heat. A high selectivity of flotation with a steam-air mixture can be explained using the concepts of a phonon component of disjoining pressure, the value and sign of which are associated with a difference in the dynamic structure of liquid in the wetting film and bulk liquid.

How to cite: Evdokimov S.I., Gerasimenko T.E. Determination of rational steam consumption in steam-air mixture flotation of apatite-nepheline ores // Journal of Mining Institute. 2022. Vol. 256. p. 567-578. DOI: 10.31897/PMI.2022.62
Metallurgy and concentration
  • Date submitted
    2022-04-20
  • Date accepted
    2022-07-21
  • Date published
    2022-11-03

Iron ore beneficiation technologies in Russia and ways to improve their efficiency

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Increasing the efficiency of crushing circuits is associated with a decrease in the particle size of finely crushed ore and the use of dry magnetic separation of crushed ore. Reducing grinding costs is achieved by using drum mills jointly with mills of other designs. The use of automation systems, slurry demagnetization, technologies with staged concentrate separation, and beneficiation and fine screening in a closed grinding cycle lead to a reduction in grinding costs. The main industrial technology for improving the quality of concentrate is its additional beneficiation using regrinding, fine screening, flotation, and magnetic-gravity separators. Increasing the integrated use of iron ore raw materials is associated with an increase in the yield of iron concentrate and the production of hematite concentrate during the beneficiation of hematite-magnetite ores and ilmenite concentrate during the beneficiation of titanomagnetite ores. Incremented concentrate yield is possible by using magnetic separators with an increased magnetic induction up to 0.25-0.5 T in the first stages of beneficiation. To obtain hematite and ilmenite concentrates, combined technologies can be used, including fine screening, high-gradient magnetic, gravity, flotation, and electrical separation.

How to cite: Pelevin A.E. Iron ore beneficiation technologies in Russia and ways to improve their efficiency // Journal of Mining Institute. 2022. Vol. 256. p. 579-592. DOI: 10.31897/PMI.2022.61
Geology
  • Date submitted
    2022-03-22
  • Date accepted
    2022-06-15
  • Date published
    2022-07-26

Gold in biogenic apatites of the Baltic-Ladoga phosphorite basin

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The distribution of gold in biogenic apatites from the Ordovician deposits in the northwest of the East European Platform shows that the maximum concentration of gold in apatites is found within the Ladoga-Baltic suture zone. Gold mineralization has a superimposed character, which is confirmed by the dependence of the gold content on the size of apatite particles and a number of isotope geochemical systematics in biogenic apatites. Gold is present in the form of high fineness particles to 20 µm in size on the surface of biogenic apatite fragments (phosphate brachiopod shells and conodont elements) and is easily extracted. In 10 % of samples of biogenic apatites, the total content of rare earth elements is more than 1 wt.%.

How to cite: Felitsyn S.B., Alfimova N.A. Gold in biogenic apatites of the Baltic-Ladoga phosphorite basin // Journal of Mining Institute. 2022. Vol. 255. p. 470-475. DOI: 10.31897/PMI.2022.47
Metallurgy and concentration
  • Date submitted
    2021-03-12
  • Date accepted
    2021-04-12
  • Date published
    2021-06-24

Increasing the efficiency of phosphate ore processing using flotation method

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The paper presents flotation of two phosphate ore samples of different origin. Statistical analysis was used to study the effect of operating parameters on flotation efficiency. The paper proposes to increase the efficiency of flotation processing of magmatic phosphate ore with a low grade of the valuable component (P 2 O 5 = 10.88 %), containing nepheline and feldspars, by means of direct anionic flotation. Authors present an optimization of anionic flotation using tall oil fatty acids mixed with anionic phospholane as an anionic collector. The effect of adding soda ash to compensate for the influence of calcium cations on technological parameters of P 2 O 5 flotation was examined. The results of studying the flotation of nepheline ore (flotation tailings of magmatic phosphate ore) showed that replacement of phospholane with oxyethylated isotridecanol allowed to obtain a high-quality concentrate. It was estimated that with the addition of Na 2 CO 3 in the amount of 2,000 g/t, a concentrate was obtained with the grade and recovery of phosphorus pentoxide equal to 39.15 and 94.19 %, respectively. The paper proposes to increase the efficiency of flotation processing of sedimentary phosphate ore with a low grade of the valuable component (P 2 O 5 = 22.5 %), containing gypsum and quartz, by means of desliming followed by anionic or cationic reverse flotation. Tall oil fatty acid with anionic phospholane was used as a collector in anionic reverse flotation, and amine was used in cationic reverse flotation. Sodium tripolyphosphate was used as a P 2 O 5 depressant. It was found to be an effective depressant in both anionic and cationic flotation. When analyzing the statistical plan, it was estimated that the maximum grade of the valuable component in the concentrate (P 2 O 5 = 31.23 %) and the recovery to concentrate of 95.22 % were obtained in the chamber product at amine consumption of 950.88 g/t and sodium tripolyphosphate consumption of 500 g/t.

How to cite: Aleksandrova T.N., Elbendari A.M. Increasing the efficiency of phosphate ore processing using flotation method // Journal of Mining Institute. 2021. Vol. 248. p. 260-271. DOI: 10.31897/PMI.2021.2.10
Metallurgy and concentration
  • Date submitted
    2020-04-15
  • Date accepted
    2020-05-13
  • Date published
    2020-10-08

Processing of platinum group metal ores in Russia and South Africa: current state and prospects

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The presented study is devoted to a comparative review of the mineral raw material base of platinum group metals (PGMs) and technologies of their processing in South Africa and Russia, the largest PGM producers. Mineralogical and geochemical classification and industrial value of iron-platinum and platinum-bearing deposits are presented in this work. The paper also reviews types of PGM ore body occurrences, ore processing methods (with a special focus on flotation processes), as well as difficulties encountered by enterprises at the processing stage, as they increase recovery of the valuable components. Data on mineralogical features of PGM deposits, including the distribution of elements in the ores, are provided. The main lines of research on mineralogical features and processing of raw materials of various genesis are identified and validated. Sulfide deposits are found to be of the highest industrial value in both countries. Such unconventional PGM sources, as black shale, dunites, chromite, low-sulfide, chromium and titanomagnetite ores, anthropogenic raw materials, etc. are considered. The main lines of research that would bring into processing non-conventional metal sources are substantiated. Analysis of new processing and metallurgical methods of PGM recovery from non-conventional and industrial raw materials is conducted; the review of existing processing technologies for platinum-bearing raw materials is carried out. Technologies that utilize modern equipment for ultrafine grinding are considered, as well as existing reagents for flotation recovery; evaluation of their selectivity in relation to platinum minerals is presented. Basing on the analysis of main technological processes of PGM ore treatment, the most efficient schemes are identified, i.e.,gravity and flotation treatment with subsequent metallurgical processing.

How to cite: Aleksandrova T.N., О’Connor C. Processing of platinum group metal ores in Russia and South Africa: current state and prospects // Journal of Mining Institute. 2020. Vol. 244. p. 462-473. DOI: 10.31897/PMI.2020.4.9
Metallurgy and concentration
  • Date submitted
    2019-06-06
  • Date accepted
    2019-08-09
  • Date published
    2020-04-24

Studies of enrichment of sulfide and oxidized ores of gold deposits of the Aldan shield

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The paper presents the analysis of studies of the enrichment of sulfide and oxidized ores in Yakutia deposits. The ore of the deposit is a mixture of primary, mixed and oxidized ores. The main useful component of the studied ore samples is gold with a content of 1.5 to 2.8 g/t, the silver content is low – 5-17 g/t. Ore minerals are represented by sulfides, among which pyrite predominates. The total sulfide content does not exceed 3-5 %. The presence in the ore of free and associated gold with a grain size from fractions of a micron to 1.5 mm. Gold is represented by nuggets in intergrowth with sulfides and also forms independent inclusions. Ores are classified as easily cyanidable. It was found that the content of amalgamable gold is 10-49, the share of cyanidable gold ranges from 66.67-91, the share of refractory gold is 9.0-33.33 %, which in absolute amount equals to 0.24-0.8 g/t. The extraction of gold in gravitation concentrate varies depending on the gold content in the ore and the yield of concentrate and for ores with a gold content of 1.5-2.8 g/t from 40 to 60 %. The direct cyanidation of all studied ore samples established the possibility of extracting gold into solution up to 86.7-92.9 %, the gold content in cyanidation cakes is 0.2-0.3 g/t. Investigations of the gravitation concentrate by the method of intensive cyanidation showed that with an initial gold content of ~ 500 g/t, up to 98.9 % is extracted into the solution. The gold content in intensive cyanide cakes will be 6-15 g/t. A set of studies carried out by the authors of the article at various institutes showed that it is advisable to process ore from the deposit using cyanidation technology with preliminary gravitational extraction of gold.

How to cite: Fedotov P.K., Senchenko A.E., Fedotov K.V., Burdonov A.E. Studies of enrichment of sulfide and oxidized ores of gold deposits of the Aldan shield // Journal of Mining Institute. 2020. Vol. 242. p. 218-227. DOI: 10.31897/PMI.2020.2.218
Metallurgy and concentration
  • Date submitted
    2018-09-12
  • Date accepted
    2019-01-05
  • Date published
    2020-04-24

Flotation extraction of elemental sulfur from gold-bearing cakes

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Currently, in the development of the raw materials base of the gold mining industry, there is a tendency to reduce the quality of the initial mineral raw materials due to the depletion of reserves of rich gold-bearing ores. The article discusses the technology of extraction of refractory gold-bearing concentrates based on low-temperature leaching of pyrite concentrate. A decrease in the parameters of the autoclave oxidation of sulfide minerals, such as pyrite and arsenopyrite, leads to the incomplete extraction of gold into the solution and, consequently, its losses during subsequent cyanidation. As a possible option for a more complete extraction of gold using low-temperature oxidation technology, a method of flotation separation of elemental sulfur from leaching cakes is proposed. According to the basic process flow chart, the flotation process designed for gold extraction is carried out after autoclave oxidation, but before cyanidation. A series of experiments were carried out with varying reagent conditions and the dependence of gold losses on the extraction of elemental sulfur in the flotation tailings was established. As determining factors, pH and solid content in the initial pulp were considered. The paper justifies the separation of elemental sulfur from autoclave cake to enriched sulfur concentrate. The cake flotation modes after autoclave oxidative leaching of pyrite concentrate are investigated. The distribution of elemental sulfur and gold by flotation products makes it possible to conduct the tailings cyanidation process with acceptable indicators.

How to cite: Ivanik S.A., Ilyukhin D.A. Flotation extraction of elemental sulfur from gold-bearing cakes // Journal of Mining Institute. 2020. Vol. 242. p. 202-208. DOI: 10.31897/PMI.2020.2.202
Metallurgy and concentration
  • Date submitted
    2017-11-20
  • Date accepted
    2018-01-09
  • Date published
    2018-04-24

Sulfidization of silver-polymetallic ores of «Goltsovoe» deposit for decreasing loss of silver in mill tailings

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The results of laboratory studies of flotation concentration of silver-polymetallic ores of the Goltsovoe deposit at the Omsukchansk concentrator are presented. The results of sieve analysis of mill tailings of the experimental sample of MTP N 101 (N 7577-i) are described. They indicate that a large amount of silver (123 g/t) is lost in the size class – 0.040 mm (yield 50.25 %). According to the results of mineralogical analysis, it is established that the major losses of noble metal are associated with its fine impregnation in oxides, sulfides and silicate rocks. The main silver-bearing minerals are acanthite, polybasite and kustelite (class – 0.040 mm). Experimental studies were carried out in two stages. The purpose of the first stage is to determine the influence of grinding fineness in flotation feed (for a finished class content of 0.074 mm in the range of 60-95 %) for silver recovery at different amounts of butyl potassium xanthate (50, 150, 300 g/t). The purpose of the second stage is to evaluate the effectiveness of sulfidization at different consumption of sodium sulfide Na 2 S·9H 2 O (50, 150, 200, 450, 750 g/t – 1 % aqueous solution) under the conditions of the optimal reagent mode established in the first stage of the study. The results of experiments to determine the optimum grinding fineness and studies on the enrichment of silver-polymetallic ore with the use of sodium sulfide as a sulfidizer are presented. The efficiency of the sulfidization process is estimated. The following experimental dependencies of silver recovery are established: on the degree of grinding and consumption of butyl potassium xanthate; on variations of grinding fineness and the consumption of sodium sulphide (with a consumption of butyl xanthate 150 g/t); and on grinding fineness at optimum consumption of sodium sulfide 150 g/t and butyl potassium xanthate 300 g/t. A comparative evaluation of dependence of silver recovery index from the degree of grinding fineness before and after introduction of sodium sulphide (collecting agent consumption of 150 g/t) is given. T\

How to cite: Shumilova L.V., Kostikova O.S. Sulfidization of silver-polymetallic ores of «Goltsovoe» deposit for decreasing loss of silver in mill tailings // Journal of Mining Institute. 2018. Vol. 230. p. 160-166. DOI: 10.25515/PMI.2018.2.160
Metallurgy and concentration
  • Date submitted
    2015-10-19
  • Date accepted
    2015-12-27
  • Date published
    2016-08-22

Key directions in processing carbonaceous rocks

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Mathematical statistics techniques and the data from laboratory mineral and technological studies of samples were used to identify the most common natural and technological associations of microelements in carbonaceous rocks which could be of industrial value if extracted in the form of commercial products. The discovered structures of spheroidal and ring ferrocarbonaceous clusters are respective formations of the class of metal fullerens with expressed magnetic properties. Such clusters may serve as construction blocks for new magnetic structures since each of them is a separate magnetic domain. Extracting such structures and their practical use opens the way to future technologies. It is expected to employ such results in the future in the course of designing new techniques and technologies for benefication of carbonaceous raw materials while developing comprehensively solid mineral resources in the mining industry regions of Russia.

How to cite: Aleksandrova T.N. Key directions in processing carbonaceous rocks // Journal of Mining Institute. 2016. Vol. 220. p. 568-572. DOI: 10.18454/PMI.2016.4.568
Metallurgy and concentration
  • Date submitted
    2015-07-26
  • Date accepted
    2015-09-12
  • Date published
    2016-02-24

Technological aspects of extraction of precious and rare metals from carbonaceous rocks

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The results of mineralogical, geochemical and technological research of black shale rocks are given. It is proved that black shales are now regarded as a new promising and innovative source of precious and rare-metal raw materials. It is pointed out that 3 wt. % of black shales samples is colloid-salt fraction (nanofraction) with a particle size less than 1000 nm and it can be extracted with water under specially chosen conditions. The use of water instead of chemically active reagents guarantees the absence of dissolved mineral matrix and clearly shows the colloidal salt component in samples. The results determine the direction of creating some new methods and technologies of carbonaceous feed dressing for integrated development of solid minerals in the mining and oil producing regions of Russia.

How to cite: Aleksandrova T.N., Panova E.G. Technological aspects of extraction of precious and rare metals from carbonaceous rocks // Journal of Mining Institute. 2016. Vol. 217. p. 72-79.
Metallurgy and concentration
  • Date submitted
    2014-11-24
  • Date accepted
    2015-01-02
  • Date published
    2015-10-26

Complex processing of apatite-nepheline ores based on the creation of closed-loop process flow sheets

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The article presents the chemical and engineering fundamentals of processing apatite and nepheline concentrates directly on the Kola Peninsula. Implementation of the existing separate processing of nepheline and apatite concentrates demonstrates inefficiency of these technologies due to the formation of waste calcium sulfate and calcium silicate, which have so far not found a practical use and are wastes stored in sludge repositories of the Russian Federation. Suggested new scientific and technical solutions will allow enterprises to significantly increase the volume of production of new in-demand marketable products due to rational and complex use of mineral raw materials of the Kola Peninsula, reduce their costs while decreasing the volume of rock extraction and eliminate waste creating a closed-loop technological cycle of processing apatite and nepheline ores.

How to cite: Alekseev A.I. Complex processing of apatite-nepheline ores based on the creation of closed-loop process flow sheets // Journal of Mining Institute. 2015. Vol. 215. p. 75-82.
Economics and management
  • Date submitted
    2009-08-10
  • Date accepted
    2009-10-14
  • Date published
    2010-02-01

Prospects of development of open society «Apatite»

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Prospects of development of Open Society «Apatit» – the basic supplier of raw materials for manufacture of mineral fertilizers in Russia are considered. The rational actions connected with increase of a production efficiency on Open Society «Apatit» are offered.

How to cite: Noskov V.A., Gurev A.A. Prospects of development of open society «Apatite» // Journal of Mining Institute. 2010. Vol. 186. p. 227-229.