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sample preparation artifacts

Geotechnical Engineering and Engineering Geology
  • Date submitted
    2023-04-13
  • Date accepted
    2023-10-25
  • Date published
    2025-02-25

Assessment of the ecological state of aquatic ecosystems by studying lake bottom sediments

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The article presents the results of coupled palynological and geochemical studies of five various genesis lakes, located along the route of the expedition “In the footsteps of Alexander von Humboldt in Siberia, Altai and Eastern Kazakhstan”, dedicated to the double anniversary: the 190th anniversary of the expedition across Russia of the famous scientist and his 250th birthday. A geochemical analysis of water and bottom sediments of Ik Lake (Siberia), Lakes Kolyvanskoe and Beloe (Altai), Lake Bezymyannoe (Kazakhstan) and Nagornyi Pond (Altai) was carried out. Based on their results an assessment of studied lakes ecological state was given through single and integral criteria. A high level of pollution was noted for Nagornyi Pond and Lake Bezymyannoe, which is caused by a significant technogenic load from nearby mines. This is consistent with the data of palynological research. The aquatic ecosystems of Lakes Kolyvanskoe and Beloe are characterized by a satisfactory ecological situation, but they experience an increased recreational load. The results of spore-pollen analysis and analysis of non-pollen palynomorphs showed the low ability of these lakes to self-healing. The most favorable ecological state and high self-cleaning capacity were noted for Lake Ik, which is consistent with the data of palynological studies. It is being confirmed with the results of palynological studies. It was therefore concluded about the ability to make a quick assessment of the aquatic ecosystems’ ecological state by studying lakes using coupled palynological and geochemical analysis.

How to cite: Chukaeva M.A., Sapelko T.V. Assessment of the ecological state of aquatic ecosystems by studying lake bottom sediments // Journal of Mining Institute. 2025. Vol. 271. p. 53-62. EDN IXRSRC
Geotechnical Engineering and Engineering Geology
  • Date submitted
    2022-10-31
  • Date accepted
    2023-04-21
  • Date published
    2024-02-29

Study of the properties and action of polyelectrolytes in the treatment of the dressing plant’s discharges

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The organization of intrafactory water circulation at mining and processing enterprises, when production wastes and discharges are not sent to an external tailings dump, is an urgent environmental and economic task. Returning even a part of water into the technological process after preliminary treatment will significantly reduce the volume of polluted water discharged into tailings, which will reduce energy costs for waste transportation and the negative environmental impact. One of the wastes sent to the tailings during the ore dressing wastes from the Kovdor deposit to the tailings dump is the discharge of thickeners for the preparation of apatite flotation feed. In order to choose the effective discharge cleaning regime, the authors have evaluated the action of polyacrylamide flocculants. It has been discovered that the apatite and calcite particles interact more effectively with the anionic flocculant. This fact determines its advantage for the treatment of suspended particles. The influence of the residual concentration of a flocculant on the apatite flotation, where a part of the returned treated water goes, has been assessed. Compared to flotation with recycled water, there is a decrease of P2O5 extraction into apatite concentrate of equal quality. In order to obtain the required enrichment indicators on the treated water, it is necessary to adjust the collector (tall oil fatty acids) and depressor (liquid glass) costs.

How to cite: Mitrofanova G.V., Chernousenko E.V., Artemev A.V., Pospelova Y.P., Smirnova N.A., Barmin I.S. Study of the properties and action of polyelectrolytes in the treatment of the dressing plant’s discharges // Journal of Mining Institute. 2024. Vol. 265. p. 95-103. EDN CVUHNQ
Geotechnical Engineering and Engineering Geology
  • Date submitted
    2022-03-14
  • Date accepted
    2022-06-20
  • Date published
    2022-11-10

Model of a walking sampler for research of the bottom surface in the subglacial lake Vostok

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Technologies and technical means for investigation of subglacial lakes in Antarctic is a new developing scientific and technical direction, which today has no clearly established methodology. Based on the developed technology of drilling a new access well to lake Vostok and its penetration as well as analysis of existing methods and devices for bottom sediment sampling, a basic model of a sampler with a walking-type mover, capable of moving along different trajectories and operating in a wide technological range, is proposed. The proposed device model is equipped with different actuators for sampling the bottom surface with different physical and mechanical properties. Based on the presented basic model of the walking sampler, a mathematical model of the device was developed, which was based on the theoretical mechanics methods. As a result of conducted research the dependencies were obtained, which allow making a scientifically justified choice of optimal values for geometric and force parameters of the walking sampler. A conceptual design of the walking sampler has been developed, taking into account the mutual location and coupling of its main components, the overall dimensions of the delivery tool, as well as the esthetic component of the device.

How to cite: Shishkin E.V., Bolshunov A.V., Timofeev I.P., Avdeev A.М., Rakitin I.V. Model of a walking sampler for research of the bottom surface in the subglacial lake Vostok // Journal of Mining Institute. 2022. Vol. 257. p. 853-864. DOI: 10.31897/PMI.2022.53
Metallurgy and concentration
  • Date submitted
    2022-04-13
  • Date accepted
    2022-05-25
  • Date published
    2022-11-03

Mineralogical and technological features and patterns of selective disintegration of ferruginous quartzites of the Mikhailovskoye deposit

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The growing demand for ferrous metallurgy products necessitates the introduction of technologies that increase the efficiency of the processing of iron-bearing raw materials. A promising trend in this area is the implementation of solutions based on the possibility of selective disintegration of ores. The purpose of this work was to establish the laws of selective disintegration of ferruginous quartzites based on the results of the study of mineralogical and technological properties of raw materials. We present data on the study of mineralogical and technological features of ferruginous quartzites of the Mikhailovskoye deposit. The data were obtained using X-ray fluorescence analysis and automated mineralogical analysis. Based on studies of the nature of dissemination and the size of grains of rock-forming and ore minerals, the tasks of ore preparation are formulated. The parameters for the iron and silicon oxide distribution by grain-size classes in the grinding products were established during the study. Based on empirical dependences, the grain size of grinding was predicted, at which the most effective release of intergrowths of ore minerals and their minimum transition to the size class of –44 µm should be achieved.

How to cite: Aleksandrova T.N., Chanturiya A.V., Kuznetsov V.V. Mineralogical and technological features and patterns of selective disintegration of ferruginous quartzites of the Mikhailovskoye deposit // Journal of Mining Institute. 2022. Vol. 256. p. 517-526. DOI: 10.31897/PMI.2022.58
Metallurgy and concentration
  • Date submitted
    2021-03-31
  • Date accepted
    2022-04-26
  • Date published
    2022-11-03

Features of obtaining metallurgical products in the solid-state hydride synthesis conditions

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A scientific substantiation of solid-phase feedstock choice and preparation has been carried out, and the thermodynamic and kinetic aspects of solid-state hydride synthesis (SHS) of metal products have been analyzed using the nickel dichloride reduction as an example. The preliminary dehydration modes and methods for controlling the complete removal of crystalline water from chloride raw materials and Olenegorsk superconcentrate, which is natural oxide raw material, are described. Conditions, including initial solid chloride particle sizes, are established under which diffusion complications of reduction to metal in methyldichlorosilane vapor are minimized. Thermodynamic estimates of nickel chlorides and oxides reduction possibility, iron and copper with ammonia and methane at temperatures of 400-1000 K in equilibrium conditions have been carried out. It has been shown that the stoichiometric coefficients of the nickel dichloride in ammonia overall reduction reaction calculated by thermodynamic modeling are in agreement with experimental data. In contrast to the copper dichloride reduction, for nickel dichloride the formation of metal monochloride at the intermediate stage is uncharacteristic, which is associated with a higher thermal stability of nickel dichloride. The main kinetic regularities of the reduction of nickel, copper, and iron to metal under SHS conditions in ammonia, monosilane, and methane, as well as the nickel dichloride with methyldichlorosilane vapor and methane successive reduction, are considered. Approximation of experimental data by topochemical equations in a linear form showed that for reduction degrees a up to 0.7-0.8, these data are satisfactorily described by the Roginsky – Schultz equation. For a > 0,8 the “shrinking sphere” model works better, which confirms the localization of the solid-state reduction reaction at the interface, moves deep into the crystal with the formation of a of interlocked metal germs. The importance and prospects of the results obtained for the theory development of metallurgical processes, deep complex processing of natural iron oxide raw materials, metal products and new generation materials production, including superhydrophobic ones, are discussed. The relevance of the study from the point of view of applying the method of physical and chemical analysis to the study of complex heterogeneous metallurgical processes is noted.

How to cite: Syrkov A.G., Yachmenova L.A. Features of obtaining metallurgical products in the solid-state hydride synthesis conditions // Journal of Mining Institute. 2022. Vol. 256. p. 651-662. DOI: 10.31897/PMI.2022.25
Metallurgy and concentration
  • Date submitted
    2020-06-29
  • Date accepted
    2021-05-21
  • Date published
    2021-09-20

Transformation of grains of technological raw materials in the process of obtaining fine powders

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Crushing and grinding of materials are the most common processes of sample preparation for subsequent analysis and industrial application. Recently, grinding has become one of the most popular methods for producing nano-sized powders. This study investigates certain features of grain transformation in the process of grinding ores with finely dispersed valuable components in order to liberate them, as well as specifics of grinding metallurgical raw materials, metals and their mixtures for using them as initial components in metallurgical and other technological processes. We identified and examined structural and morphological changes of various powders after ultrafine grinding using the methods of scanning electron microscopy and X-ray microanalysis. It was proved that in order to take into account sample preparation artifacts during analytic studies of solid samples and development of technological processes, fine grinding of heterogeneous materials, especially if they contain metals, requires monitoring of the ground product by methods of scanning electron microscopy and X-ray microanalysis.

How to cite: Gembitskaya I.M., Gvozdetskaya M.V. Transformation of grains of technological raw materials in the process of obtaining fine powders // Journal of Mining Institute. 2021. Vol. 249. p. 401-407. DOI: 10.31897/PMI.2021.3.9
Oil and gas
  • Date submitted
    2020-12-02
  • Date accepted
    2021-04-21
  • Date published
    2021-06-24

Modeling the processes of deformation and destruction of the rock sample during its extraction from great depths

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Article investigates the change in the geophysical properties of rocks in the process of extracting the rock sample from great depths. Evaluation of changes in effective elastic properties, porosity and permeability of rock samples during extraction was carried out by means of finite element modeling. Assessment of the critical dimensions and orientation of internal defects, leading to the destruction of the rock samples during extraction from great depths, has been made based on the methods of linear destruction mechanics. Approach that makes it possible to calculate the change in the mechanical properties, porosity and fracturing of reservoir rocks in the process of extracting the rock sample from depths to the surface is proposed. Use of refined data on the mechanical properties of recoverable rock samples makes it possible to increase the accuracy of digital geological models required for geological exploration, determination of reservoir properties and oil and gas saturation of a field, and development of oil and gas deposits. Application of such models is especially relevant at all stages of the fields development with hard-to-recover reserves.

How to cite: Grishchenko A.I., Semenov A.S., Melnikov B.E. Modeling the processes of deformation and destruction of the rock sample during its extraction from great depths // Journal of Mining Institute. 2021. Vol. 248. p. 243-252. DOI: 10.31897/PMI.2021.2.8
Oil and gas
  • Date submitted
    2019-10-30
  • Date accepted
    2020-02-03
  • Date published
    2020-10-08

Concept of technology for determining the permeability and porosity properties of terrigenous reservoirs on a digital rock sample model

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The aim of the article is to form the concept of technology for determining the permeability and porosity properties of terrigenous reservoirs using mathematical modeling methods on a digital rock sample model. Digital rock sample modeling is used to assess geological oil reserves. The article presents the concept of digital rock sample modeling technology, which allows carrying out qualitative investigations to determine the permeability and porosity characteristics of the formation, including modeling the pore space and filtration processes. The essence of the concept is that the simulation model of the microstructure for the digital model is formed on the basis of a large number of parameters obtained during lithological and petrographic investigations of thin sections, a study of the sludge and geophysical investigations of wells. The acquired model can be used as a basis for subsequent modeling of filtration processes. Conductivity of single channels of the formed model can be calculated using molecular dynamics methods, models of Boltzmann's lattice equations, and other mathematical models and methods. Based on the results of the study carried out, the application of stochastic packing methods for modeling the structure of the pore space in the digital rock sample model of terrigenous reservoirs is substantiated. In connection with the development of computer and nanotechnologies and their use in the oil and gas industry, solutions that allow obtaining adequate results of digital rock sample models are of high importance and relevance for the production sector. It is especially important to use digital rock sample models in the study of reservoir rocks of shelf fields in the western part of the Russian Arctic, oil shales, rocks represented by loose weakly cemented reservoirs, and others, which are complex for physical experiments.

How to cite: Belozerov I.P., Gubaydullin M.G. Concept of technology for determining the permeability and porosity properties of terrigenous reservoirs on a digital rock sample model // Journal of Mining Institute. 2020. Vol. 244. p. 402-407. DOI: 10.31897/PMI.2020.4.2
Electromechanics and mechanical engineering
  • Date submitted
    2018-10-28
  • Date accepted
    2018-12-30
  • Date published
    2019-04-23

Development and research of formation technologies on specialized presses with subsequent sintering of high-density details from iron-based powders

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Creating shifts of the lyaers in a deforming workpieces improves the quality of the product produced by pressure treatment. qual-channel angular pressing and precipitations of a cylindrical billet with a rotating turnaround were developed by specialists earlier and became basic for scientists engaged in nanotechnology. One of the most modern schemes for creating nanostructures by processing on presses is the «Cyclic Extrusion Compression» scheme (in Russia – «Hourglass»), which has significant drawbacks. To date, research on the creation of layer shifts in compacted metal powders is substantially less than in compaction of compact blanks. The article developed compaction schemes for presses of blanks from iron-based powders that have a certain analogy with the «Hourglass», while lacking the disadvantages inherent in the named scheme and implemented on the created samples of specialized hydraulic presses. The results of the studies of density, strength and microhardness before sintering the samples molded from a number of domestic and imported powders on iron base, including those doped with carbon and other alloying components, are described. It has been established that with the use of the formation schemes for powders providing large shifts between particles, the density of the preforms increases on average by 10-12 %. With an average stress (16.32 MPa) of the transverse section of the molded specimen prior to its sintering, molding with shifts between particles increases this stress by 78 %. The strength after sintering of samples made using the compaction schemes developed by the authors of the article increases approximately by 2 times. Magnetic pulse treatment (MPT) of a molded sample prior to its sintering increases its resistance to shearing before sintering, regardless of the molding pattern. When MPT of both the powder and the molded sample is executed, the most uniform distribution of microhardness in the sample is achieved, and after subsequent sintering, the most uniform distribution of the mechanical characteristics of the product. The results of all studies are described by regression equations.

How to cite: Dmitriev A.M., Korobov N.V., Badalyan A.Z. Development and research of formation technologies on specialized presses with subsequent sintering of high-density details from iron-based powders // Journal of Mining Institute. 2019. Vol. 236. p. 216-228. DOI: 10.31897/PMI.2019.2.216
Oil and gas
  • Date submitted
    2018-05-20
  • Date accepted
    2018-07-07
  • Date published
    2018-10-24

Justification of representative data volume of porosity and permeability properties for obtaining statistically reliable petrophysical connections

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The article discusses the issues of justifying the data volume for a petrophysical description of an object based on the results of traditional laboratory measurements, as well as X-ray tomography data processing. A new approach to the calculation of porosity and permeability properties of reservoirs with the data of the X-ray tomography method by forming an array of virtual cubes is considered. The issues of required number of allocated cubes for fluid dynamics modeling are discussed. The criteria for the number of laboratory measurements and virtual cubes derived from a digital model for obtaining statistically reliable petrophysical connections are shown. Paper concludes that it is necessary to correctly compare the calculated and laboratory petrophysical connections.

How to cite: Abrosimov A.A., Shelyago E.V., Yazynina I.V. Justification of representative data volume of porosity and permeability properties for obtaining statistically reliable petrophysical connections // Journal of Mining Institute. 2018. Vol. 233. p. 487-491. DOI: 10.31897/PMI.2018.5.487
Oil and gas
  • Date submitted
    2018-01-01
  • Date accepted
    2018-03-24
  • Date published
    2018-06-22

Complex petrophysical correction in the adaptation of geological hydrodynamic models (on the example of Visean pool of Gondyrev oil field)

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The authors review a method of combined porosity and volume density correction in the process of modeling the distribution of reservoir permeability. Basing on petrophysical investigations of core samples from Bashkir fold deposits, an association between rock porosity, density and permeability has been analyzed. Significant correlation has been observed for the above mentioned parameters in porous collectors in contrast to reduced correlation for dense rocks and intervals of anomalously high poroperm characteristics. For terrigene porous collectors the authors propose a model of permeability assessment based on combined porosity and density correction. A modified model was developed for Visean pool of Gondyrev oil field, where collector permeability had been calculated as a function of rock porosity and density. The modified model has been compared to the conventional one; significant differences have been detected. In the modified version maximum permeability is associated with the southern part of the pool, whereas the conventional method points out the central part and predicts lowering permeability closer to the periphery. Geological model in the modified version is more homogenous than the conventional one and has no sharp peaks and valleys. The calculations have been made that reproduce the history of field development for both permeability volumes. Authors demonstrate that total oil production obtained using the modified model has a much better correlation with the actual data. The best results from using suggested method apply to the initial stage of development due to better convergence of high-rate wells. On the whole, comparison of two methods shows that for the purposes of production history adaptation the modified model is significantly better than the conventional one. Hence, the method of density correction allows for better justification of differences in the lithology of Visean collectors, which ultimately results in higher accuracy of data on residual oil reserves in the deposit.

How to cite: Repina V.A., Galkin V.I., Galkin S.V. Complex petrophysical correction in the adaptation of geological hydrodynamic models (on the example of Visean pool of Gondyrev oil field) // Journal of Mining Institute. 2018. Vol. 231. p. 268-274. DOI: 10.25515/PMI.2018.3.268
Mining
  • Date submitted
    2016-11-21
  • Date accepted
    2017-01-23
  • Date published
    2017-04-14

Prospects of obtaining samples of bottom sediments from subglacial lake Vostok

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The paper proves the timeliness of obtaining and examining bottom sediments from subglacial Lake Vostok. Predictive geological section of Lake Vostok and information value of bottom sediments have been examined. Severe requirements towards environmental security of lake examinations and sampling of bottom sediments rule out the use of conventional drilling technologies, as they would pollute the lake with injection liquid from the borehole. In order to carry out sampling of bottom sediments from the subglacial lake, it is proposed to use a dynamically balanced tool string, which enables rotary drilling without any external support on borehole walls to transmit counter torque. A theoretical analysis has been carried out to assess the operation of the tool string, which is a two-mass oscillatory electromechanical system of reciprocating and rotating motion (RRM) with two degrees of freedom.

How to cite: Vasilev N.I., Leichenkov G.L., Zagrivnyi E.A. Prospects of obtaining samples of bottom sediments from subglacial lake Vostok // Journal of Mining Institute. 2017. Vol. 224. p. 199-208. DOI: 10.18454/PMI.2017.2.199
Metallurgy and concentration
  • Date submitted
    2015-07-07
  • Date accepted
    2015-09-16
  • Date published
    2016-02-24

Activation of heap leaching of low-sulfide ores the invisible gold

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This article deals with a physical-chemical model of heap leaching processes justifying new technological approaches to recovering dispersed forms of gold from ores, placer sands and deute-rogene mineral raw materials. The key process of this model includes lattice diffusion of high-energy hydrion minerals and hydroxyl-radicals formed as a result of photochemical and electro-chemical processing of initial reagent aqueous solutions. Active components of gas-water emulsions obtained while processing initial reagent solutions provide a structural and material trans-formation of a mineral lattice which concentrates clusters of dispersed gold creating conditions for its interacting with complexing compounds of process solutions. The article also considers the technological processes of activation heap leaching of dispersed gold from the Pogromnoe ore field and the results of the experiments conducted in percolators with their charge ranged from 3 to 100 kg. The results have proved the efficiency of using gas-water suspensions prepared in the pho-toelectrochemical reactor with active ion-radical oxidizing agents.

How to cite: Sekisov A.G., Rubtsov Y.I., Lavrov A.Y. Activation of heap leaching of low-sulfide ores the invisible gold // Journal of Mining Institute. 2016. Vol. 217. p. 96-101.
Mining
  • Date submitted
    2014-12-30
  • Date accepted
    2015-02-03
  • Date published
    2015-12-25

Open mining technique for unconventional mineral deposits

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Nowadays the majority of deposits are successfully exploiting by mining enterprises with the help of traditional excavation and loading equipment. Typically, metals, construction materials, etc. are mined and extracted on these deposits, but modern society is progressing and producing new requirements to metals properties for creating a new type of equipment. The metals with new properties are located in unconventional areas: either in technogenic deposits (overburden dumps, tailings, etc.) or in hard-to-get natural formations. Technogenic mines, being a tailing of Kachkanarsky mining and processing plant, are referred to such unique deposits, which have expensive metals (scandium, gallium, strontium, titanium), as well as the natural deposit – rhenium deposit, located in the crater of an active volcano. Potentialities of open mining in the largest rhenium deposit with complex environmental occurrence have been analyzed in the paper. Temperature measurement results of adjacent strata and a temperature scheme of the host rocks on a separate site and the entire field have been presented. An open mining technique for a primary mining area as well as perspective methods of rock preparation for excavation, applicable to this particular deposit, has been considered.

How to cite: Kholodnyakov G.A., Argimbaev K.R. Open mining technique for unconventional mineral deposits // Journal of Mining Institute. 2015. Vol. 216. p. 82-88.
Problems in geodynamic safety in the exploration of solid deposits
  • Date submitted
    2009-10-13
  • Date accepted
    2009-12-29
  • Date published
    2010-09-22

Assessment of the level of technological production of coal reserves in mine fields with intensive mining of fiat-lying coal seams

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The levels of technological production of coal reserves in the stoping faces have been determined depending on the main determining factors, such as suitability of conditions, their preparation and equipment of longwalls.

How to cite: Baranov S.G., Rozenbaum M.A. Assessment of the level of technological production of coal reserves in mine fields with intensive mining of fiat-lying coal seams // Journal of Mining Institute. 2010. Vol. 188. p. 43-46.
Problems in geomechanics of technologeneous rock mass
  • Date submitted
    2009-07-06
  • Date accepted
    2009-09-24
  • Date published
    2010-04-22

Investigation of geomechanical processes in underground mining of mineral resources at the automated test bench for physical modeling

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The paper presents the particular results of development of the method for modeling on equivalent materials in the recent years, concerning the evolution of the primary technical base of the laboratory – test benches, which allowed to supplement substantially the potentialities of physical modeling for its complex application jointly with the full-scale and mathematical methods in solving a number of actual tasks in mining geomechanics.

How to cite: Zuev B.Y. Investigation of geomechanical processes in underground mining of mineral resources at the automated test bench for physical modeling // Journal of Mining Institute. 2010. Vol. 185. p. 85-88.
Drilling
  • Date submitted
    2008-10-11
  • Date accepted
    2008-12-19
  • Date published
    2009-12-11

The development of the effective method for sampling of native-state core in natural gashydrate deposits

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Gas hydrates – the firm crystal connections of water and low-molecular waterproof natural gases such as carbohydrates (mainly methane), СО 2 , N 2 and others. At present, time exploitation of the Messoyahsk (Russia) and Mallik (Canada) deposits of gas hydrates is conducted actively. The further perfection of prospecting methods in the field of studying gas hydrate containing sediments in round extent depends on improvement of methods for native-state core sampling from these sediments.

How to cite: Chistyakov V.K. The development of the effective method for sampling of native-state core in natural gashydrate deposits // Journal of Mining Institute. 2009. Vol. 183. p. 311-317.
Geology, search and prospecting of mineral deposits
  • Date submitted
    2008-10-06
  • Date accepted
    2008-12-10
  • Date published
    2009-12-11

Appearance of entropy principle in distribution оf the gold mass while formation of minable gold mineralization

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The rule of the entropy distributiveness for mass of the metal in gold ores is detected at different scale levels. This regularity is resulted as a consequence of redistribution of the gold and host rocks after their primary conditions. Revealing of those rules may allow reviewing the notions on nature and genesis of gold mineralizaition.

How to cite: Sendek S.V. Appearance of entropy principle in distribution оf the gold mass while formation of minable gold mineralization // Journal of Mining Institute. 2009. Vol. 183. p. 112-126.