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U-Pb изотопное датирование

Geology
  • Date submitted
    2023-11-10
  • Date accepted
    2024-05-02
  • Date published
    2025-04-25

Paleoproterozoic Saltakh Pluton, Anabar Shield: mineralogical composition, age and a geodynamic setting

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The Saltakh Massif is located in the northern Anabar Shield, in the Saltakh shear-zone. It consists of two-pyroxene schists and plagiogneisses metamorphosed under granulite-facies conditions. Their chemical composition is consistent with that of a differentiated series of rocks ranging from gabbro to tonalites with abundant alaskitic gneissose granite veins and bodies. The rocks are mainly high-potassium (K2O/Na2O > 0.50), high-magnesium (mg# 50-70), low-titanium (TiO2 0.35-1.31 wt.%) with low TiO2 concentration in clino- and orthopyroxene. Normative olivine makes up 6-9 % of metagabbroic rocks. The rocks display well-defined negative Ti, Nb, Ta, and P anomalies typical of subduction magmatism. The two-pyroxene gneisses show high Sr/Y ratios of 67.6-88 and (La/Yb)N of 24.8-25.6. Saltakh rocks are part of a shoshonite series, as indicated by Nb/La, La/Yb, Th/Nb and Ce/Yb ratios. All the rocks display positive εNd(T) values of 1.9-4.1 and εSr(T) of 0.77-17.8 indicative of a mantle source of magma and T(Nd)DM of 2,20-2,26 Ga. U-Pb zircon dating (SHRIMP II) has shown that the protoliths of Saltakh melanocratic rocks were dated at 2100-2086 Ma, and those of two-pyroxene plagiogneisses of tonalite composition were dated at 2025±7 Ma. Alaskitic gneissose granites were dated at 1969±7 Ma. The study of the trace element composition of zircon has revealed general enrichment in LREE. High LREE concentrations are due to secondary zircon alterations and the shoshonitic pattern of the melt, the high-temperature conditions of crystallization, and an anomalous fluid regime. The geodynamic setting in which the Saltakh Massif was formed was consistent with a pericontinental magmatic arc. The formation of alaskitic gneissose granites was due to anatexis provoked by later collision processes. Saltakh magmatic rocks were formed simultaneously with magmatic rocks from the Khapchan prospect which occur farther south, and were studied earlier (2095±10 Ma tholeiitic metadiorites and 2030±17 Ma calc-alkaline metatonalites). We interpret them as part of a metamorphosed juvenile Paleoproterozoic suprasubduction complex.

How to cite: Gusev N.I., Romanova L.Y. Paleoproterozoic Saltakh Pluton, Anabar Shield: mineralogical composition, age and a geodynamic setting // Journal of Mining Institute. 2025. Vol. 272 . p. 16-39. EDN SRITGO
Geology
  • Date submitted
    2023-11-02
  • Date accepted
    2024-03-05
  • Date published
    2024-08-26

The polyphase Belokurikhinsky granite massif, Gorny Altai: isotope-geochemical study of zircon

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Based on the isotopic-geochemical analyses of zircons from granites of the Belokurikhinsky massif in the Gorny Altai using the U-Pb method, the ages of three intrusion phases have been determined for the first time: the age of the first phase refers to the time interval of 255-250 Ma, the second and the third phases have similar ages of about 250 Ma. The formation time of the Belokurikhinsky massif is estimated as not exceeding 5-8 Ma. The δ18O values for zircons from granites of the second and the third intrusion phases average around 11.5-12.0 ‰, indicating a significant contribution of a crustal component in the formation of the parent melts for granites of these phases. The crystallization temperature values of the zircons by the Ti-in-zircon thermometer for three phases range from 820 to 800 °C. The P-T crystallization parameters of titanite from the first phase, determined using a titanite thermobarometer, average around 770 °C and 2.7 kbar. The zircons from the first phase mostly exhibits geochemical characteristics of typical magmatic zircons. The zircons from the second and the third intrusion phases either may be unaltered magmatic zircons or enriched in incompatible elements (LREE, Th, U, Ti, Ca, etc.) due to fluid influence, resembling hydrothermal-metasomatic type zircons in terms of their geochemical characteristics. A number of zircon grains from the second and the third phases of granites demonstrate anomalous geochemical characteristics – the REE distribution spectra atypical for zircons (including “bird's wing” type spectra with oppositely tilted of light and heavy REE distribution profiles), as well as significantly higher contents of certain trace elements compared to other varieties. Such an enriched zircon composition and wide variations in the incompatible element content are due to non-equilibrium conditions of zircon crystallization and evolution of the fluid-saturated melt composition during the final stages of the massif formation.

How to cite: Skublov S.G., Levashova E.V., Mamykina M.E., Gusev N.I., Gusev A.I. The polyphase Belokurikhinsky granite massif, Gorny Altai: isotope-geochemical study of zircon // Journal of Mining Institute. 2024. Vol. 268 . p. 552-575. EDN RGKCIJ
Geology
  • Date submitted
    2023-02-07
  • Date accepted
    2023-06-20
  • Date published
    2024-02-29

Origin of carbonate-silicate rocks of the Porya Guba (the Lapland-Kolvitsa Granulite Belt) revealed by stable isotope analysis (δ18O, δ13C)

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Carbonate-silicate rocks of unclear origin have been observed in granulites of the Porya Guba of the Lapland-Kolvitsa Belt within the Fennoscandinavian Shield. The present work aims to reconstruct possible protoliths and conditions of metamorphic transformation of these rocks based on oxygen and carbon isotopic ratios combined with phase equilibria modeling. Isotope analysis and lithochemical reconstructions suggest that carbonate-silicate rocks of the Porya Guba represent metamorphosed sediments (possibly marls) with the isotopic composition corresponding to the Precambrian diagenetically transformed carbonates (δ18O ≈ 17.9 ‰, SMOW and δ13C ≈ –3.4 ‰, PDB). The chemical composition varies depending on the balance among the carbonate, clay, and clastic components. Significant changes of the isotopic composition during metamorphism are caused by decomposition reactions of primary carbonates (dolomite, siderite, and ankerite) producing CO2 followed by degassing. These reactions are accompanied by δ18O and δ13C decrease of calcite in isotopic equilibrium with CO2 down to 15 ‰ (SMOW) and –6 ‰ (PDB), respectively. The isotopic composition is buffered by local reactions within individual rock varieties, thus excluding any pronounced influence of magmatic and/or metasomatic processes.

How to cite: Krylov D.P., Klimova E.V. Origin of carbonate-silicate rocks of the Porya Guba (the Lapland-Kolvitsa Granulite Belt) revealed by stable isotope analysis (δ18O, δ13C) // Journal of Mining Institute. 2024. Vol. 265 . p. 3-15. EDN GISHQG
Geology
  • Date submitted
    2022-02-24
  • Date accepted
    2022-05-25
  • Date published
    2022-07-26

Litsa uranium ore occurrence (Arctic zone of the Fennoscandian Shield): new results of petrophysical and geochemical studies

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Mineralogical, petrophysical and geochemical studies have been carried out to determine the sequence and formation conditions of uranium mineralization within the Litsa ore occurrence (Kola Region). Mineralogical studies show the following formation sequence of ore minerals: uraninite – sulfides – uranophane, coffinite, pitchblende. Two stages of uranium mineralization are distinguished: Th-U (1.85-1.75 Ga) and U (400-300 Ma). The distribution of physical properties of rocks in the area is consistent with the presence of two temporal stages in the formation of mineralization with different distribution and form of uranium occurrence in rocks. The factors that reduce rock anisotropy are the processes of migmatization and hydrothermal ore mineralization, which heal pores and cracks. Fluid inclusions in quartz studied by microthermometry and Raman spectroscopy contain gas, gas-liquid and aqueous inclusions of different salinity (1.7-18.4 wt.% NaCl-eq.). According to homogenization temperatures of inclusions in liquid phase, the temperature of the Paleoproterozoic and Paleozoic stages of uranium mineralization at the Litsa ore occurrence is ~ 300 and 200 °С, respectively. Correlations of the spatial distribution of elastic anisotropy index with an elevated radioactive background allow using this petrophysical feature as one of the prognostic criteria for uranium and complex uranium mineralization when carrying out uranium predictive work.

How to cite: Il’chenko V.L., Afanasieva E.N., Kaulina T.V., Lyalina L.M., Nitkina E.A., Mokrushina O.D. Litsa uranium ore occurrence (Arctic zone of the Fennoscandian Shield): new results of petrophysical and geochemical studies // Journal of Mining Institute. 2022. Vol. 255 . p. 393-404. DOI: 10.31897/PMI.2022.44
Geology
  • Date submitted
    2022-03-20
  • Date accepted
    2022-05-25
  • Date published
    2022-07-26

Ophiolite association of Cape Fiolent (western part of the Mountainous Crimea) – the upper age constraint according to the U-Pb isotope dating of plagiorhyolites (Monakh Cliff)

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The article presents the results of U-Pb isotope dating (SHRIMP-II, VSEGEI, Saint Petersburg) of zircon crystals extracted from plagiorhyolites of the Monakh Cliff in the area of Cape Fiolent in the western part of the Mountainous Crimea (southern suburb of Sevastopol). a concordant age estimate of 168.3±1.3 Ma was obtained from 20 zircon crystals. It exactly corresponds to the Bajocian/Bathonian boundary of the Middle Jurassic according to the International Chronostratigraphic Chart (February 2022 version). The available results of isotope dating of igneous rocks from the Mountainous Crimea, as well as their geochemical typification are synthesised. The plagiorhyolites of the Monakh Cliff in the area of Cape Fiolent are spatially, and most likely paragenetically, associated with the wallrock (Cape Vinogradny) and ore (Heraclea Plateau on the cognominal peninsula) massive sulphide formations, as well as pillow basalts, gabbroids, and serpentinized hyperbasites, combined into the ophiolite association of Cape Fiolent. The obtained dating is the upper age limit for the entire ophiolite association of Cape Fiolent.

How to cite: Kuznetsov N.B., Romanyuk T.V., Strashko A.V., Novikova A.S. Ophiolite association of Cape Fiolent (western part of the Mountainous Crimea) – the upper age constraint according to the U-Pb isotope dating of plagiorhyolites (Monakh Cliff) // Journal of Mining Institute. 2022. Vol. 255 . p. 435-447. DOI: 10.31897/PMI.2022.37
Geology
  • Date submitted
    2022-04-11
  • Date accepted
    2022-06-15
  • Date published
    2022-07-26

Magma feeding paleochannel in the Monchegorsk ore region: geochemistry, isotope U-Pb and Sm-Nd analysis (Kola region, Russia)

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A comprehensive study of a 340 m thick lenticular-sheet body of ultramafic composition penetrated by structural well M-1 at a depth of about 2.2 km was accomplished. Its main volume is composed of plagioharzburgite; fine-grained rocks of norite and orthopyroxenite chilling zones are preserved on endocontacts. The rocks of the body are similar in composition to the rocks near the underlying ore-bearing layered intrusion – the Monchepluton. The age of intrusion of the ultramafic body is 2510 ± 9 Ma (U-Pb, ID-TIMS, zircon) and, taking into account analytical errors, is comparable with the formation period of the Monchepluton (2507-2498 Ma). According to the study of the Sm-Nd system in rocks and minerals, a positive value of the e Nd (+1.1) parameter was established, similar to that in dunites and chromitites of the Monchepluton. Based on these results, the ultramafic body penetrated at depth was assigned to the magma feeding paleochannel through which the ultramafic, weakly contaminated magma entered the overlying magma chamber. This body is a unique example of a magma-feeding system for the ore-bearing layered intrusion of Precambrian age.

How to cite: Smolkin V.F., Mokrushin A.V., Bayanova T.B., Serov P.A., Ariskin A.A. Magma feeding paleochannel in the Monchegorsk ore region: geochemistry, isotope U-Pb and Sm-Nd analysis (Kola region, Russia) // Journal of Mining Institute. 2022. Vol. 255 . p. 405-418. DOI: 10.31897/PMI.2022.48
Geology
  • Date submitted
    2022-04-18
  • Date accepted
    2022-05-25
  • Date published
    2022-07-26

U-Pb (SHRIMP-RG) age of zircon from rare-metal (Li, Cs) pegmatites of the Okhmylk deposit of the Kolmozero-Voron’ya greenstone belt (northeast of the Fennoscandian shield)

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The results of isotopic and geochronological study of zircon from rare-metal pegmatites of the Okhmylk deposit are presented. There were no reliable data on the age of lepidolite-spodumene-pollucite pegmatites of this and the other deposits spatially located within the Archean Kolmozero-Voron’ya greenstone belt. The earlier estimates of the pegmatite age indicate a broad time range from 2.7 to 1.8 Ga. Zircon in the studied pegmatites is characterized by inner heterogeneity, where core and rim zones are distinguished. Minor changes are observed in the core zones, they have a spotted structure and contain numerous uranium oxide inclusions. According to X-ray diffraction analysis, zircon crystallinity is preserved completely in these areas. Complete recrystallization with modification of the original U-Pb isotopic system occurred in the zircon rims. New U-Pb (zircon) isotopic and geochronological data of 2607±9 Ma reflect the time of crystallization of pegmatite veins in the Okhmylk deposit. Isotopic data with ages of ~1.7-1.6 Ga indicate later hydrothermal alteration. The obtained results testify to the Neo-Archean age of the formation of the Okhmylk deposit 2.65-2.60 Ga, reflecting the global age of pegmatite formation and associated the world's largest rare-metal pegmatite deposits.

How to cite: Kudryashov N.M., Udoratina O.V., Kalinin A.A., Lyalina L.M., Selivanova E.A., Grove M.J. U-Pb (SHRIMP-RG) age of zircon from rare-metal (Li, Cs) pegmatites of the Okhmylk deposit of the Kolmozero-Voron’ya greenstone belt (northeast of the Fennoscandian shield) // Journal of Mining Institute. 2022. Vol. 255 . p. 448-454. DOI: 10.31897/PMI.2022.41
Geology
  • Date submitted
    2021-08-05
  • Date accepted
    2021-11-30
  • Date published
    2021-12-27

Morozkinskoye gold deposit (southern Yakutia): age and ore sources

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The paper presents the results of the comprehensive isotope geochemical (Re-Os, Pb and δ 34 S) study of sulfide mineralization of the Morozkinskoye deposit. The ore zones of the deposit are localized in the syenite massif of Mount Rudnaya, which is located within the Central Aldan ore region (southern Yakutia). Gold mineralization is represented by vein-disseminated or vein type mineralization and is manifested in acidic low-temperature metasomatites – beresites (Qz-Ser-Ank-Py). For the first time we obtained an age estimate of the gold mineralization ~ 129 ± 3 Ma, which the synchronism of the hydrothermal ore process in the beresites, which formed the Morozkinskoye deposit, and magmatic crystallization of the syenites of Mount Rudnaya (~130 Ma). The osmium initial isotopic composition of the studied sulfides indicates a mixed mantle-crustal source of sulfide mineralization. New lead isotopic data of syenites indicate the predominance of mantle lead and an insignificant role of the lower – crust lead, while the isotopic composition of pyrite denotes the presence of the upper crustal material in the ore genesis. The sulfide δ 34 S values vary from –2.3 to +0.6 ‰ and indicate a predominantly magmatic source of sulfur in the ores.

How to cite: Guzev V.E., Terekhov A.V., Krymsky R.S., Belyatsky B.V., Molchanov A.V. Morozkinskoye gold deposit (southern Yakutia): age and ore sources // Journal of Mining Institute. 2021. Vol. 252 . p. 801-813. DOI: 10.31897/PMI.2021.6.3
Geology
  • Date submitted
    2020-05-28
  • Date accepted
    2020-05-28
  • Date published
    2020-06-30

The age of mineralization of Mayskoe gold ore deposit (Central Chukotka): results of Re-Os isotopic dating

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The article presents the results of the sulfide mineralization dating of the Mayskoe gold ore deposit using the Re-Os isotope system and isochron age estimation method of the main sulfide minerals: arsenopyrite, pyrite, and antimonite. The complex multistage formation of the studied sulfides, as well as the close intergrowths of genetically different mineral phases, did not allow obtaining a single rhenium-osmium isochron corresponding to the formation time of sulfide mineralization. Isochrones for single minerals, collected from each sulfide sample, turned out to be the result of isotopically distinct components mixture (radiogenic crustal and non-radiogenic mantle) and do not make sense from the geochronological point of view. In terms of geology, the most significant result of the study is an age estimation of 128.8 ± 4.4 Ma, obtained for the sulfide mineralization of Mayskoe deposit using Re-Os isotope dating of single fractions of pyrite and antimonite of the ore mineralization stage. While arsenopyrite is most closely associated with gold mineralization, one of the arsenopyrite varieties corrodes framboidal pyrite of the pre-ore stage, has a maximum of the crust component in the osmium isotopic composition and forms a mixing line in the isochron diagram with an apparent formation age of 458 ± 18 Ma. The initial osmium isotopic composition of the studied sulfides indicates a mixed mantle-crust source of sulfide mineralization. The issue of simultaneous ore genesis and granitoid magmatism in the Mayskoe deposit remained unresolved (the age of granitoids according to the U-Pb zircon system is 108 Ma). However, a possible solution could be the further determination of the Re-Os isochron age of the ore mineralization sulphides from the single paragenesis of a specific sample containing both arsenopyrite and pyrite (+ antimonite) with gold.

How to cite: Artemiev D.S., Krymsky R.S., Belyatsky B.V., Ashikhmin D.S. The age of mineralization of Mayskoe gold ore deposit (Central Chukotka): results of Re-Os isotopic dating // Journal of Mining Institute. 2020. Vol. 243 . p. 266-278. DOI: 10.31897/PMI.2020.3.266
Geology
  • Date submitted
    2017-09-02
  • Date accepted
    2017-11-22
  • Date published
    2018-02-22

Age and metamorphic conditions of the granulites from Capral-Jegessky synclinoria, Anabar shield

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The paper presents the results of the isotope, geochemical and thermobarometric study of plagio-crystalline schist containing in the Upper Anabar series of the Anabar Shield. Granulite complexes of the paleoplatforms are the most important issue in addressing the fundamental problem of the Earth's crust origin and its composition. The early stages of crust formation which correspond to the deeply metamorphosed rocks of the platform basements, available for study within the shields, are of particular interest. The study of the age and metamorphic conditions of granulites by the case of the Upper Ananbar series allows specifying the stages the Anabar Shield's ancient crust formation. Isotope-geochemical (U-Pb geochronology for zircon and Sm-Nd for garnet-amphibole-WR) and thermoba-rometric (Theriak-Domino) studies of plagio-crystalline schist allowed to identify two Paleoproterozoic metamorphism stages within the territory of the Anabar Shield with an age of about 1997 and 1919 million years. The peak conditions of granulite metamorphism are determined as 775±35 С and 7.5±0.7 kbar, the parameters of the regressive stage are 700  C and 7 kbar. The sequence of the rocks metamorphic transformations can be assumed: high-thermal metamorphism of the granulite facies (T ≤ 810  C) and subsequent sub-isobaric (about 7 kbar) cooling to 700  C with a water activity increase and formation of Grt-Amp paragenesis corresponding to the transition from the granulite to amphibolite facies. Data on the REE and other trace elements distribution in zircon and rock-forming minerals obtained by the ion microprobe analysis contribute significantly to the isotope-geochemical data interpretation.

How to cite: Sergeeva L.Y., Berezin A.V., Gusev N.I., Skublov S.G., Melnik A.E. Age and metamorphic conditions of the granulites from Capral-Jegessky synclinoria, Anabar shield // Journal of Mining Institute. 2018. Vol. 229 . p. 13-21. DOI: 10.25515/PMI.2018.1.13
Oil and gas
  • Date submitted
    2015-10-23
  • Date accepted
    2015-12-19
  • Date published
    2016-08-22

Nondestructive techniques to control the quality and quantity of oil flows

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The article considers the issue of improving the efficiency of exploiting the acting oil fields and transportation system on the basis of modern hi-tech technologies to control the extracted and transported material. Factors are studied that lower the reliability of oil flow measurements, both qualitatively and quantitatively, the main ambiguities are described of using current systems for metrological account of oil transported through the pipelines. The effect is studied of inclusions in the transported oil flow on measurement efficiency. A technique is suggested for selective measurements of separate phases in the complex multi-phase flows with isotropic radio emission, the principal relationships are presented to describe the intensity of direct and scattered gamma-radiation on flow parameters. Criteria are given for developing a measurement system that would control the actual component composition of the flow with time, hence the amount of oil transported; that would enable organizing a centralized open department to control the quality of oil and transportation conditions, upgrade the level of production and provide high measurement accuracy. Results are presented of testing the technique on an operating oil field; the relative error margin of measuring free gas content was 0.2 %. The range is reviewed of possible applications for the measurement system of multi-phase multi-component flows, developed in the Saint Petersburg Mining University.

How to cite: Proskuryakov R.M., Kopteva A.V. Nondestructive techniques to control the quality and quantity of oil flows // Journal of Mining Institute. 2016. Vol. 220 . p. 564-567. DOI: 10.18454/PMI.2016.4.564