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Geotechnical Engineering and Engineering Geology
  • Date submitted
    2024-04-24
  • Date accepted
    2024-09-24
  • Date published
    2024-11-12

Study and justification of the combination of beneficiation processes for obtaining flake graphite from technogenic carbon-containing dusts

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The most important task of modern production development is to provide the mineral and raw materials sector of the economy with resources included in the list of strategic raw materials, including flake graphite. In addition to natural raw materials, the source of its obtaining can be metallurgical production wastes not involved in processing. Development of metallurgical dust beneficiation technology will solve the problem of obtaining high-purity flake graphite with a crystal structure close to ideal and in demand in the production of high-tech materials. It will allow creating a renewable raw material base of graphite and utilising metallurgical production wastes. The research included the study of dust beneficiation by coarseness, magnetic and flotation methods, the influence of dust disintegration processes on beneficiation indicators. Based on the established technological properties of the components of dusts, magnetic, flotation and gravity beneficiation methods can be applied for their separation in different sequence. It is shown that dusts from different sites have different enrichability by these methods, and it should be taken into account when developing a complex technology of their processing. The degree of beneficiation increases in a row of dusts from the blast furnace shop (BF) – electric steel smelting shop (ESS) – oxygen-converter shop (OCS). The method of grinding has a significant influence on the separation indicators – at dry grinding in a centrifugal-impact mill with subsequent pneumatic classification the quality of graphite concentrates increases by 22.7 % of carbon for BF dust and by 13.48 % of carbon for ESS dust. OCS dust beneficiation indicators are high at coarse grinding with steel medium – mass fraction of carbon 96.1 %.

How to cite: Orekhova N.N., Fadeeva N.V., Musatkina E.N. Study and justification of the combination of beneficiation processes for obtaining flake graphite from technogenic carbon-containing dusts // Journal of Mining Institute. 2024. Vol. 269 . p. 777-788. EDN UNUYXS
Geotechnical Engineering and Engineering Geology
  • Date submitted
    2023-05-17
  • Date accepted
    2023-08-17
  • Date published
    2023-10-27

Scientific and technical substantiation of the possibility for the organization of needle coke production in Russia

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Russia is one of the world's leading steel producers, while about 33 % of production comes from the scrap remelted in arc steelmaking furnaces. The graphitized electrodes of SHP and UHP grades, mainly consisting of needle coke, are used for high current loads and temperatures in furnaces. USA, Japan, Korea, and China are focused on needle coke production, where coal (tar and pitch) and petroleum (decantoil), by-products of metallurgical factories and oil refineries, are used as raw materials. Russia's annual demand for needle coke is approximately 100 thousand tons, but all of it is covered by imports. Russia's raw material potential, established by the authors of the article, is more than 5 million tons per year and includes decantoil, coal tar and pitch, and heavy pyrolysis tar. The results of obtaining needle coke from decantoil and heavy pyrolysis tar are given below. The prototypes of needle coke were produced on specially designed delayed coking laboratory units (loading up to 0.25 and 80 kg). Raw materials were modified according to the original technology of Saint Petersburg Mining University, the convergence of target properties of which is confirmed by the results of quality analysis of the obtained needle coke, including after 100-fold scaling. The electrodes were molded from the obtained coke. After standardized stages of firing, mechanical processing and graphitization at 2,800-3,000 °C, the coefficient of linear thermal expansion was less than 1 × 10–6 К–1, and the value of specific electrical resistance was 7.1-7.4 μOhm, which proves that the obtained carbon material corresponds in quality to Japanese analogues and Super Premium needle coke.

How to cite: Rudko V.А., Gabdulkhakov R.R., Pyagai I.N. Scientific and technical substantiation of the possibility for the organization of needle coke production in Russia // Journal of Mining Institute. 2023. Vol. 263 . p. 795-809. EDN KYNHWL
Geology
  • Date submitted
    2009-08-11
  • Date accepted
    2009-10-07
  • Date published
    2010-02-01

Mineralogical and geochemical features of metamorphic roks of Pestpaksha (Kola peninsula)

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The rock composition was studied, the garnet composition was researched with a X-ray phase analysis, and equilibrium pressures of the garnet crystallization were calculated with the geobarometer GASP, thermal properties of graphite were characterized and polymorphic modification was identified by X-rays diffraction.

How to cite: Kurguzova A.V. Mineralogical and geochemical features of metamorphic roks of Pestpaksha (Kola peninsula) // Journal of Mining Institute. 2010. Vol. 186 . p. 27-30.