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Vol 50 Iss. 3
Pages:
94-100
Download volume:
RUS
Article

On the state of molybdenum and tungsten in acid solutions extracted by amines

Authors:
M. A. Petrov
V. V. Dolivo-Dobrovolsky
Date submitted:
1969-12-06
Date accepted:
1970-02-03
Date published:
1970-07-10

Abstract

Molybdenum and tungsten can be extracted with alkylamines from acidic solutions obtained during the chemical refinement of scheelite concentrate at the Tyrnyauz Processing Plant. These solutions contain 5-8 g/l of molybdenum and tungsten. Each is present in both oxidized and reduced forms. The solution also contains significant amounts of phosphorus and silicon. Apparently, molybdenum and tungsten are found in these solutions in the form of phosphoric and silicic heteropoly acids, since these metals are excellently extracted by solutions of amines in nonpolar diluents. To determine the state of molybdenum and tungsten in these solutions, the behavior of metals during extraction by their amines from hydrochloric acid solutions in the presence of phosphorus and silicon in a wide range of hydrochloric acid concentrations was studied...

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References

  1. Petrov M. A., Maslenitsky N. N., Davydova A.D. Extraction of molybdenum and tungsten from acidic solutions. Non-ferrous Metals, No. 3, 1967.
  2. Klitina V. I., Sudakov F. P., Alimarin I. N. Extraction of reduced phosphoric-molybdenum acid by high-molecular-weight amines. J. Analytical. Chemistry, vol. XXI, issue 3, 1966.
  3. Yatsimirskiy K. B., Alekseeva I. I. Study of absorption spectra and determination of dissociation constants of molybdenum acid. Univ. Proc. Chemistry and Chemical Technology, vol. I, issue 1, 1958.
  4. Yadimirsky K. B., Alekseeva I. I. On the state of molybdenum acid in slightly acidic solutions. J. Inorganic. Chemistry, vol. 1, issue 4, 1959.
  5. Alekseeva I. I. Study of polymerization of molybdenum acid by kinetic method. J. Inorganic. Chemistry, vol. XII, issue 7, 1967.
  6. Babko A. K., Gridina G. I. Polviones of molybdenum in acidic solutions. J. Inorganic. Chemistry, vol. XIII, issue 1, 1968.
  7. Nabivanets B. I. On the issue of the isoelectric point of molybdenum acid. J. Inorganic Chemistry, vol. XIII, issue 3, 1968.
  8. Babko A. K., Nabivanets B. I. Study of the state of molybdates in solution. I. Motion of ions during electrolysis. Solubility of molybdenum anhydride. J. Inorganic. Chemistry, vol. II, issue 9, 1957.
  9. Babko A. K., Nabivanets B. I. Study of the state of molybdates in solution. II. Absorption of molybdenum by ionites. J. inorganic. Chemistry, V. I., iss, P. 9, 1957.
  10. Alimarin I. P., Sudakov F. P., Klitii a V. I. Extraction of heteropoly compounds and its application in inorganic analysis. Successes of Chemistry, vol. XXXIV, vol. 8, 1965.

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