Ключевые слова

2411-3336

2541-9404

Записки Горного института

Journal of Mining Institute

Санкт-Петербургский горный университет императрицы Екатерины ΙΙ

Empress Catherine II Saint Petersburg Mining University

QOALPE

pmi-16282

https://pmi.spmi.ru/pmi/article/view/16282

Геология

Geology

A new insight into recording the mineral composition of carbonate reservoirs at well killing: experimental studies

Новый взгляд на учет минерального состава карбонатных коллекторов при глушении скважин: экспериментальные исследования

Chernykh

Vasilii I.

Черных

В. И.

Chernykh

Vasilii I.

Vasily.Chernykh@pnn.lukoil.com

0000-0001-8152-0048

Филиал ООО «ЛУКОЙЛ-Инжиниринг» «ПермНИПИнефть» в г. Перми (Пермь, Россия) Branch of OOO “LUKOIL-Engineering” “PermNIPIneft” in Perm (Perm, Russia)

Martyushev

Dmitrii A.

Мартюшев

Д. А.

Martyushev

Dmitrii A.

martyushevd@inbox.ru

0000-0002-5745-4375

Пермский национальный исследовательский политехнический университет (Пермь, Россия) Perm National Research Polytechnic University (Perm, Russia)

Ponomareva

Inna N.

Пономарева

И. Н.

Ponomareva

Inna N.

pin79@yandex.ru

0000-0003-0546-2506

11 04 2024

2024

270 893 903 07 07 2023 27 12 2023 25 12 2024

2024

В. И. Черных, Д. А. Мартюшев, И. Н. Пономарева

Vasilii I. Chernykh, Dmitrii A. Martyushev, Inna N. Ponomareva

Эта статья доступна по лицензии Creative Commons Attribution 4.0 International (CC BY 4.0)

This article is licensed under a Creative Commons Attribution 4.0 International License (CC BY 4.0)

https://pmi.spmi.ru/pmi/article/view/16282

Важным технологическим этапом перед проведением капитального или текущего ремонта скважин остается операция по глушению, в процессе которой происходит проникновение фильтрата в призабойную зону пласта. Воздействие технологических жидкостей и их фильтрата на горную породу оказывает существенное влияние на фильтрационно-емкостные свойства карбонатных коллекторов, которые снижаются по причине миграции мелких частиц. Известно немного научных исследований, изучавших процесс взаимодействия фильтрата жидкости глушения с карбонатной горной породой и миграцию мелких частиц. В наших экспериментах использовалась водная фаза, которая является основой для глушения скважин в чистом виде, для приготовления блокирующих составов и используется в системе поддержания пластового давления. С образцами керна, отобранными из продуктивной части коллектора, моделировался процесс глушения скважины с созданием пластовых термобарических условий. Фильтрат жидкости глушения выдерживался в течение семи суток, что характеризует среднее время проведения ремонтных работ на добывающих скважинах месторождений Пермского края. С использованием микрорентгеновской томографии и сканирующего электронного микроскопа получены изображения до и после эксперимента, которые позволили установить факт снижения общего количества пустот из-за миграции мелких частиц и, как следствие, снижение проницаемости образцов. Измерение pH и концентрации частиц в водной фазе выполнено до и после эксперимента и свидетельствует о минеральных реакциях, которые произошли в результате растворения горной породы. Результаты проведенных экспериментов позволили установить снижение проницаемости карбонатных образцов в среднем на 50 %, обусловленное кольматацией пустотного пространства и миграцией мелких частиц (глинистые и неглинистые).

Well killing operation remains an important technological stage before well workover or servicing, during which filtrate penetrates the bottomhole area of the formation. The impact of process fluids and their filtrate on rock has a significant influence on permeability and porosity of carbonate reservoirs, which decrease due to fines migration. There are few known scientific studies of the interaction of killing fluid filtrate with carbonate rock and fines migration. In our experiments, an aqueous phase was used which is the basis for well killing in pure form, for the preparation of blocking agents and is used in reservoir pressure maintenance system. Core samples taken from the pay of the reservoir were used to simulate the well killing process with generation of reservoir thermobaric conditions. Killing fluid filtrate was kept for seven days, which characterizes the average workover time at flowing wells in the fields of the Perm Territory. Using micro-X-ray tomography and scanning electron microscope, images were obtained before and after the experiment, which allowed confirming a decrease in total number of voids due to fines migration and, as a consequence, a decreasing permeability of samples. Measurement of pH and fines concentration in the aqueous phase was performed before and after the experiment and pointed to mineral reactions occurring as a result of rock dissolution. The results of experiments made it possible to record a decrease in permeability of carbonate samples by an average of 50 % due to clogging of void space and migration of fines (clayey and non-clayey).

Ключевые слова мелкие частицы растворение микрорентгеновская томография сканирующий электронный микроскоп проницаемость глинистые минералы низкоминерализованная вода

Keywords fines dissolution micro-X-ray tomography scanning electron microscope permeability clay minerals low mineralized water

Исследования выполнены при поддержке Министерства науки и высшего образования Российской Федерации (проект № FSNM-2024-0005).

The research was conducted with support of the Ministry of Science and Higher Education of the Russian Federation (project N FSNM-2024-0005).

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