2411-3336 2541-9404 Записки Горного института Journal of Mining Institute Санкт-Петербургский горный университет императрицы Екатерины ΙΙ Empress Catherine II Saint Petersburg Mining University 10.31897/PMI.2022.92 pmi-15780 https://pmi.spmi.ru/pmi/article/view/15780 Autoclave modeling of corrosion processes occurring in a gas pipeline during transportation of an unprepared multiphase medium containing CO2 Автоклавное моделирование коррозионных процессов, происходящих в газопроводе при транспортировке неподготовленной многофазной среды, содержащей CO2 Shaposhnikov Nikita О. Шапошников Н. О. Shaposhnikov Nikita О. Shaposhn_no@spbstu.ru 0000-0003-3542-2492 Санкт-Петербургский политехнический университет Петра Великого (Россия) Saint Petersburg Polytechnic University of Peter the Great (Russia) Golubev Ivan A. Голубев И. А. Golubev Ivan A. golubev_ia@spbstu.ru 0000-0001-7516-3566 Санкт-Петербургский политехнический университет Петра Великого (Россия) Saint Petersburg Polytechnic University of Peter the Great (Russia) Khorobrov Svyatoslav V. Хоробров С. В. Khorobrov Svyatoslav V. horobrov_sv@spbstu.ru 0000-0002-6861-4338 Санкт-Петербургский политехнический университет Петра Великого (Россия) Saint Petersburg Polytechnic University of Peter the Great (Russia) Kolotiy Alexander I. Колотий А. И. Kolotiy Alexander I. kolotij_ai@spbstu.ru 0000-0002-8072-5620 Санкт-Петербургский политехнический университет Петра Великого (Россия) Saint Petersburg Polytechnic University of Peter the Great (Russia) Ioffe Andrey V. Иоффе А. В. Ioffe Andrey V. ioffeav@its-samara.com 0000-0003-1378-7749 Инжиниринговая компания ООО «ИТ-Сервис» (Россия) Engineering company OOO “IT-Service” (Russia) Revyakin Viktor А. Ревякин В. А. Revyakin Viktor А. nadzor@its-samara.com 0000-0002-0885-6060 Инжиниринговая компания ООО «ИТ-Сервис» (Россия) Engineering company OOO “IT-Service” (Russia) 29 12 2022 2022 258 915 923 25 03 2022 06 09 2022 29 12 2022 © Nikita О. Shaposhnikov, Ivan A. Golubev, Svyatoslav V. Khorobrov, Alexander I. Kolotiy, Andrey V. Ioffe, Viktor А. Revyakin 2022 Н. О. Шапошников, И. А. Голубев, С. В. Хоробров, А. И. Колотий, А. В. Иоффе, В. А. Ревякин Nikita О. Shaposhnikov, Ivan A. Golubev, Svyatoslav V. Khorobrov, Alexander I. Kolotiy, Andrey V. Ioffe, Viktor А. Revyakin CC BY 4.0 https://pmi.spmi.ru/pmi/article/view/15780

Рассматривается проблема подбора способа обеспечения надежности функционирования объектов транспорта неподготовленного флюида в условиях присутствия углекислого газа. Углекислотная коррозия является одним из опасных видов повреждения промысловых и магистральных трубопроводов. Показано, что при проведении постановочных лабораторных испытаний с целью определения интенсивности протекания углекислотной коррозии и выбора оптимального способа защиты необходимо проводить динамические автоклавные испытания. Выдвинута и подтверждена гипотеза о несовершенстве существующих общепризнанных подходов к проведению динамических коррозионных испытаний. Предложена методика проведения испытаний, основанная на применении автоклава с верхнеприводной мешалкой, разработанного с использованием элементов математического моделирования. Потоки, создаваемые в автоклаве, обеспечивают коррозионный износ поверхности образца подобно износу внутренних поверхностей элементов трубопроводов обвязки газоконденсатных скважин. Автоклав позволяет моделировать влияние органической фазы на скорость протекания и характер коррозионных поражений поверхности металла, а также влияние скорости вращения мешалки и, соответственно, касательного напряжения сечения на скорость коррозии в присутствии/отсутствии ингибитора коррозии. Приведенные результаты постановочных испытаний позволяют судить о высокой эффективности разработанной методики испытаний.

The problem of selecting a method for ensuring the reliability of the unprepared fluid transport facilities of an unprepared fluid in the presence of carbon dioxide is considered. Carbon dioxide corrosion is one of the dangerous types of damage to field and main pipelines. It has been shown that dynamic autoclave tests should be carried out during staged laboratory tests in order to determine the intensity of carbon dioxide corrosion and to select the optimal method of protection. A hypothesis about the imperfection of the existing generally accepted approaches to dynamic corrosion testing has been put forward and confirmed. A test procedure based on the use of an autoclave with an overhead stirrer, developed using elements of mathematical modeling, is proposed. The flows created in the autoclave provide corrosive wear of the sample surface similar to the internal surfaces elements wear of the pipelines piping of gas condensate wells. The autoclave makes it possible to simulate the effect of the organic phase on the flow rate and the nature of corrosion damage to the metal surface, as well as the effect of the stirrer rotation speed and, accordingly, the shear stress of the cross section on the corrosion rate in the presence/absence of a corrosion inhibitor. The given results of staged tests make it possible to judge the high efficiency of the developed test procedure.

 Ключевые слова углекислотная коррозия динамические испытания автоклав с мешалкой автоклавные испытания физическое моделирование защита от коррозии выбор способа обеспечения надежности Keywords carbon dioxide corrosion dynamic tests autoclave with stirrer autoclave tests physical modeling corrosion protection choice of method to ensure reliability Litvinenko V. The Role of Hydrocarbons in the Global Energy Agenda: The Focus on Liquefied Natural Gas // Resources. 2020. Vol. 9. Iss. 5. № 59. DOI: 10.3390/resources9050059 Litvinenko V. The Role of Hydrocarbons in the Global Energy Agenda: The Focus on Liquefied Natural Gas. Resources. 2020. Vol. 9. Iss. 5. N 59. DOI: 10.3390/resources9050059 Tcvetkov P., Cherepovitsyn A., Makhovikov A. Economic assessment of heat and power generation from small-scale liquefied natural gas in Russia // Energy Reports. 2020. Vol. 6 (2). P. 391-402. DOI: 10.1016/j.egyr.2019.11.093 Tcvetkov P., Cherepovitsyn A., Makhovikov A. Economic assessment of heat and power generation from small-scale liquefied natural gas in Russia. Energy Reports. 2020. Vol. 6 (2), p. 391-402. DOI: 10.1016/j.egyr.2019.11.093 Zhukovskiy Y.L., Batueva D.E., Buldysko A.D. et al. Fossil Energy in the Framework of Sustainable Development: Analysis of Prospects and Development of Forecast Scenarios // Energies. 2021. Vol. 14 (17). № 5268. DOI: 10.3390/en14175268 Zhukovskiy Y.L., Batueva D.E., Buldysko A.D. et al. Fossil Energy in the Framework of Sustainable Development: Analysis of Prospects and Development of Forecast Scenarios. Energies. 2021. Vol. 14 (17). N 5268. DOI: 10.3390/en14175268 Cherepovitsyn A., Rutenko E., Solovyova V. Sustainable Development of Oil and Gas Resources: A System of Environmental, Socio-Economic, and Innovation Indicators // Journal of Marine Science and Engineering. 2021. Vol. 9 (11). № 1307. DOI: 10.3390/jmse9111307 Cherepovitsyn A., Rutenko E., Solovyova V. Sustainable Development of Oil and Gas Resources: A System of Environmental, Socio-Economic, and Innovation Indicators. Journal of Marine Science and Engineering. 2021. Vol. 9 (11). N 1307. DOI: 10.3390/jmse9111307 Цветков П.С., Федосеев С.В. Анализ специфики организации проектов малотоннажного производства СПГ // Записки Горного института. 2020. Т. 246. С. 678-686. DOI: 10.31897/PMI.2020.6.10 Tsvetkov P.S., Fedoseev S.V. Analysis of project organization specifics in small-scale LNG production. Journal of Mining Institute. 2020. Vol. 246, p. 678-686. DOI: 10.31897/ PMI.2020.6.10 Litvinenko V.S., Kozlov A.V., Stepanov V.A. Hydrocarbon potential of the Ural–African transcontinental oil and gas belt // Journal of Petroleum Exploration and Production Technology. 2017. Vol. 7 (1). P. 1-9. DOI: 10.1007/s13202-016-0248-4 Litvinenko V.S., Kozlov A.V., Stepanov V.A. Hydrocarbon potential of the Ural–African transcontinental oil and gas belt. Journal of Petroleum Exploration and Production Technology. 2017. Vol. 7 (1), p. 1-9. DOI: 10.1007/s13202-016-0248-4 Li K., Zeng Y., Luo J.L. Influence of H2S on the general corrosion and sulfide stress cracking of pipelines steels for supercritical CO2 transportation // Corrosion Science. 2021. Vol. 190. № 109639. DOI: 10.1016/j.corsci.2021.109639 Li K., Zeng Y., Luo J.L. Influence of H2S on the general corrosion and sulfide stress cracking of pipelines steels for supercritical CO2 transportation. Corrosion Science. 2021. Vol. 190. N 109639. DOI: 10.1016/j.corsci.2021.109639 Smith S.N., Joosten M.W. Corrosion of carbon steel by H2S in CO2 containing oilfield environments // CORROSION 2006, 12-16 March 2006, San Diego, California. NACE International, 2006. № 06115. Smith S.N., Joosten M.W. Corrosion of carbon steel by H2S in CO2 containing oilfield environments. CORROSION 2006, 12-16 March 2006, San Diego, California. NACE International, 2006. N 06115. Devyaterikova N., Nurmukhametova M., Kharlashin A., Popov Y. Types of corrosion damage of tubing in the oilfield // Corrosion in the Oil & Gas Industry. 2019. Vol. 121. № 03001. DOI: 10.1051/e3sconf/201912103001 Devyaterikova N., Nurmukhametova M., Kharlashin A., Popov Y. Types of corrosion damage of tubing in the oilfield.Corrosion in the Oil & Gas Industry. 2019. Vol. 121. N 03001. DOI: 10.1051/e3sconf/201912103001 АртеменковВ.Ю., КорякинА.Ю., ДикамовД.В. идр. Организация коррозионного мониторинга на объектах второго участка Ачимовских отложений Уренгойского нефтегазоконденсатного месторождения // Газовая промышленность. 2017. № S 2. С. 74-78. Artemenkov V.Yu., Koryakin A.Yu., Dikamov D.V. et al. Organization of corrosion monitoring at the facilities of the second section of the Achimov deposits of the Urengoy oil and gas condensate field. Gazovaya promyshlennost. 2017. N S 2, p. 74-78 (in Russian). Корякин А.Ю., Кобычев В.Ф., Колинченко И.В., Юсупов А.Д. Условия протекания углекислотной коррозии на объектах добычи Ачимовских отложений, методы контроля и прогнозирования // Газовая промышленность. 2017. №12 (761). С. 84-89. Koryakin A.Yu., Kobychev V.F., Kolinchenko I.V., Yusupov A.D. Conditions of the carbon dioxide corrosion on the production facilities of Achimovskie deposits, methods of monitoring and forecasting. Gazovaya promyshlennost. 2017. N 12 (761), p. 84-89 (in Russian). Алексеева Е.Л., Альхименко А.А., Ковалев М.А. и др. Оценка коррозионных свойств стальных двухслойных насосно-компрессорных труб для нефтедобычи // Материаловедение. 2021. №4. С. 10-16. DOI: 10.1134/S207511332201004X Alekseeva E.L., Alkhimenko A.A., Kovalev M.A. et al. The Evaluation of the Corrosion Properties of Steel Two-Layer Oil Well Tubing for Oil Extraction. Inorganic Materials: Applied Research. 2022. Vol. 13, p. 52-58. DOI: 10.1134/S207511332201004X Федоров А.С., Алексеева Е.Л., Альхименко А.А. и др. Исследование влияния параметров испытаний на оценку стойкости сталей к углекислотной коppозии // Заводская лаборатория. Диагностика материалов. 2021. T. 87. № 12. C. 36-41. DOI: 10.26896/1028-6861-2021-87-12-42-47 Fedorov A.S., Alekseeva E.L., Alkhimenko A.A. et al. Study of the effect of test parameters on the assessment of steel resistance to carbon dioxide corrosion. Industrial laboratory. Diagnostics of materials. 2021. Vol. 87. N 12, p. 36-41 (in Russian). DOI: 10.26896/1028-6861-2021-87-12-42-47 Choi Y.-S., Nešić S., Jung H.-G. Effect of Alloying Elements on the Corrosion Behavior of Carbon Steel in CO2 Environments // Corrosion. 2018. Vol. 74. № 5. P. 566-576. DOI: 10.5006/2705 Choi Y.-S., Nešić S., Jung H.-G. Effect of Alloying Elements on the Corrosion Behavior of Carbon Steel in CO2 Environments. Corrosion. 2018. Vol. 74. N 5, p. 566-576. DOI: 10.5006/2705 Han J. Brown B.N., Nešić S. Investigation of the Galvanic Mechanism for Localized Carbon Dioxide Corrosion Propagation Using the Artificial Pit Technique // Corrosion. 2010. Vol. 66. Iss. 9. P. 095003-095003-12. DOI: 10.5006/1.3490308 Han J. Brown B.N., Nešić S. Investigation of the Galvanic Mechanism for Localized Carbon Dioxide Corrosion Propagation Using the Artificial Pit Technique. Corrosion. 2010. Vol. 66. Iss. 9, p. 095003-095003-12. DOI: 10.5006/1.3490308 Wang Z.M., Han X., Zhang J., Wang Z.L. In situ observation of CO2 corrosion under high pressure // The International Journal of Corrosion Processes and Corrosion Control. 2014. Vol. 49. Iss. 5. P. 352-356. DOI: 10.1179/1743278213Y.0000000144 Wang Z.M., Han X., Zhang J., Wang Z.L. In situ observation of CO2 corrosion under high pressure. The International Journal of Corrosion Processes and Corrosion Control. 2014. Vol. 49. Iss. 5, p. 352-356. DOI: 10.1179/1743278213Y.0000000144 Kostitsyna I., Shakhmatov A., Davydov A. Study of corrosion behavior of carbon and low-alloy steels in CO2-containing environments // E3S Web of Conferences. 2019. Vol. 121. № 04006. DOI: 10.1051/e3sconf/201912104006 Kostitsyna I., Shakhmatov A., Davydov A. Study of corrosion behavior of carbon and low-alloy steels in CO2-containing environments. E3S Web of Conferences. 2019. Vol. 121. N 04006. DOI: 10.1051/e3sconf/201912104006 ВыбойщикМ.А., ИоффеА.В., ТетюеваТ.В. идр. Деградация и разрушение нефтегазопроводных труб в средах с высоким содержанием углекислого газа и ионов хлора // Деформация и разрушение материалов. 2020. № 4. С. 29-36. DOI: 10.31044/1814-4632-2020-4-29-36 Vyboyshchik M.A., Ioffe A.V., Tetyueva T.V. et al. Degradation and destruction of oil and gas pipes in environments with high content of carbon dioxide and chlorine ions. Deformatsiya i razrushenie materialov. 2020. Vol. 4, p. 29-36 (in Russian). DOI: 10.31044/1814-4632-2020-4-29-36 Кашковский Р.В., Ибатуллин К.А. Некоторые аспекты углекислотной коррозии стального оборудования и трубопроводов нефтегазовых промыслов // Наука и техника в газовой промышленности. 2016. № 3 (67). С. 71-91. Kashkovskii R.V., Ibatullin K.A. Some Aspects of Carbon Dioxide Corrosion of Steel Equipment and Pipelines in Oil and Gas Fields. Nauka i tekhnika v gazovoi promyshlennosti. 2016. N 3 (67), p. 71-91 (in Russian). Маркин А.Н., Низамов Р.Э. CO2-коррозия нефтепромыслового оборудования. М.: Всероссийский научно-исследовательский институт организации, управления и экономики нефтегазовой промышленности, 2003. 188 с. Markin A.N., Nizamov R.E. CO2-corrosion oilfield equipment. Moscow: Vserossiiskii nauchno-issledovatelskii institut organizatsii, upravleniya i ekonomiki neftegazovoi promyshlennosti, 2003, p. 188 (in Russian). Князькин С.А., Иоффе А.В., Выбойщик М.А., Зырянов А.О. Особенности коррозионного разрушения насосно-компрессорных труб при эксплуатации в средах с повышенным содержанием углекислого газа // Металловедение и термическая обработка металлов. 2012. № 10 (688). С. 10-14. Knyazkin S.A., Ioffe A.V., Vyboishchik M.A., Zyryanov A.O. Special features of corrosion fracture of tubing operating in media with elevated content of carbon dioxide. Metallovedenie i termicheskaya obrabotka metallov. 2012. N 10 (688), p. 10-14 (in Russian). Mazumder M.A.J., Al-Muallem H.A., Faiz M., Ali S.A. Design and synthesis of a novel class of inhibitors for mild steel corrosion in acidic and carbon dioxide-saturated saline media // Corrosion Science. 2014. Vol. 87. P. 187-198. DOI: 10.1016/j.corsci.2014.06.026 Mazumder M.A.J., Al-Muallem H.A., Faiz M., Ali S.A. Design and synthesis of a novel class of inhibitors for mild steel corrosion in acidic and carbon dioxide-saturated saline media. Corrosion Science. 2014. Vol. 87, p. 187-198. DOI: 10.1016/j.corsci.2014.06.026 Kovalev M., Alekseeva E., Shaposhnikov N. Investigation of hydroabrasive resistance of internal anti-corrosion coatings used in the oil and gas industry // IOP Conference Series: Materials Science and Engineering. 2020. Vol. 889. № 012020. DOI: 10.1088/1757-899X/889/1/012020 Kovalev M., Alekseeva E., Shaposhnikov N. Investigation of hydroabrasive resistance of internal anti-corrosion coatings used in the oil and gas industry. IOP Conference Series: Materials Science and Engineering. 2020. Vol. 889. N 012020. DOI: 10.1088/1757-899X/889/1/012020 Sun C., Liu J., Sun J. et al. Probing the initial corrosion behavior of X65 steel in CCUS-EOR environments with impure supercritical CO2 fluids // Corrosion Science. 2021. Vol. 189. № 109585. DOI: 10.1016/j.corsci.2021.109585 Sun C., Liu J., Sun J. et al. Probing the initial corrosion behavior of X65 steel in CCUS-EOR environments with impure supercritical CO2 fluids. Corrosion Science. 2021. Vol. 189. N 109585. DOI: 10.1016/j.corsci.2021.109585 Альхименко А.А., Давыдов А.Д., Харьков А.А. и др. Методы коррозионных испытаний, применяемые при разработке и промышленном освоении новых судостроительных сталей и сплавов и технологий их производства. Часть I. Лабораторные коррозионные испытания // Известия высших учебных заведений. Черная металлургия. 2022. № 65 (1). C. 48-56. DOI: 10.17073/0368-0797-2022-1-48-56 Alkhimenko A.A., Davydov A.D., Kharkov A.A. et al. Methods of ran'osion testing used for development and commercial exploitation of new shipbuilding steels and alloys. Part I. Laboratory corrosion tests. Izvestiya vysshikh uchebnykh zavedeniy. Chornaya metallurgiya. 2022. N 65 (1), p. 48-56 (in Russian). DOI: 10.17073/0368-0797-2022-1-48-56 Golubev I.A., Laptev A.B., Alekseeva E.L. et al. The effect of magnetic treatment on the effectiveness of inhibition in oilfields // E3S Web of Conferences. 2019. Vol. 121. № 02006. DOI: 10.1051/e3sconf/201912102006 Golubev I.A., Laptev A.B., Alekseeva E.L. et al. The effect of magnetic treatment on the effectiveness of inhibition in oilfields. E3S Web of Conferences. 2019. Vol. 121. N 02006. DOI: 10.1051/e3sconf/201912102006 Owen J., Ducker E., Huggan M. et al. Design of an elbow for integrated gravimetric, electrochemical and acoustic emission measurements in erosion-corrosion pipe flow environments // Wear. 2019. Vol. 428. P. 76-84. DOI: 10.1016/j.wear.2019.03.010 Owen J., Ducker E., Huggan M. et al. Design of an elbow for integrated gravimetric, electrochemical and acoustic emission measurements in erosion-corrosion pipe flow environments. Wear. 2019. Vol. 428, p. 76-84. DOI: 10.1016/j.wear.2019.03.010 Ingham B., Ko M., Kear G. et al. In situ synchrotron X-ray diffraction study of surface scale formation during CO2 corrosion of carbon steel at temperatures up to 90 °C // Corrosion Science. 2010. Vol. 52. Iss. 9. P. 3052-3061. DOI: 10.1016/j.corsci.2010.05.025 Ingham B., Ko M., Kear G. et al. In situ synchrotron X-ray diffraction study of surface scale formation during CO2 corrosion of carbon steel at temperatures up to 90 °C. Corrosion Science. 2010. Vol. 52. Iss. 9, p. 3052-3061. DOI: 10.1016/j.corsci.2010.05.025 Sk M.H., Abdullah A.M., Ko M. et al. Local supersaturation and the growth of protective scales during CO2 corrosion of steel: Effect of pH and solution flow // Corrosion Science. 2017. Vol. 126. P. 26-36. DOI: 10.1016/j.corsci.2017.05.026 Sk M.H., Abdullah A.M., Ko M. et al. Local supersaturation and the growth of protective scales during CO2 corrosion of steel: Effect of pH and solution flow. Corrosion Science. 2017. Vol. 126, p. 26-36. DOI: 10.1016/j.corsci.2017.05.026 Ingham B., Ko M., Laycock N. et al. In situ synchrotron X-ray diffraction study of scale formation during CO2 corrosion of carbon steel in sodium and magnesium chloride solutions // Corrosion Science. 2012. Vol. 56. P. 96-104. DOI: 10.1016/j.corsci.2011.11.017 Ingham B., Ko M., Laycock N. et al. In situ synchrotron X-ray diffraction study of scale formation during CO2 corrosion of carbon steel in sodium and magnesium chloride solutions. Corrosion Science. 2012. Vol. 56, p. 96-104. DOI: 10.1016/j.corsci.2011.11.017 Kermani B., Martin J.W., Esaklul K.A. Materials Design Strategy: Effects of H2S/CO2 Corrosion on Materials Selection // CORROSION 2006, 12-16 March 2006, San Diego, California. NACE International, 2006. № NACE-06121. Kermani B., Martin J.W., Esaklul K.A. Materials Design Strategy: Effects of H2S/CO2 Corrosion on Materials Selection. CORROSION 2006, 12-16 March 2006, San Diego, California. NACE International, 2006. N NACE-06121. Kermani B. Depiction of Metallurgical Parameters as Governing CO2 corrosion // CORROSION 2014, 9-13 March 2014, San Antonio, Texas, USA. NACE International, 2014. № NACE-2014-3813. Kermani B. Depiction of Metallurgical Parameters as Governing CO2 corrosion. CORROSION 2014, 9-13 March 2014, San Antonio, Texas, USA. NACE International, 2014. N NACE-2014-3813. Tröger M., Bosch C., Meuser H. et al. New alloying concepts for increased corrosion resistance of welded linepipe steels in CO2 containing aqueous media // Conference EUROCORR 2013, 1-5 September 2013, Estoril, Portugal. Tröger M., Bosch C., Meuser H. et al. New alloying concepts for increased corrosion resistance of welded linepipe steels in CO2 containing aqueous media. Conference EUROCORR 2013, 1-5 September 2013, Estoril, Portugal. Onyeji L.I., Kale G.M., Kermani M.B. Comparative Studies of the Effects of Microstructures on the Corrosion Behavior of Micro-Alloyed Steels in Unbuffered 3.5 Wt % NaCl Saturated with CO2 // International Journal of Chemical and Molecular Engineering. 2017. Vol. 11. № 2. P. 154-161. DOI: 10.5281/zenodo.1128925 Onyeji L.I., Kale G.M., Kermani M.B. Comparative Studies of the Effects of Microstructures on the Corrosion Behavior of Micro-Alloyed Steels in Unbuffered 3.5 Wt % NaCl Saturated with CO2. International Journal of Chemical and Molecular Engineering. 2017. Vol. 11. N 2, p. 154-161. DOI: 10.5281/zenodo.1128925 Bosch C., Poepperling R.K. Influence of Chromium Contents of 0.5 to 1.0 % on the Corrosion Behavior of Low Alloy Steel for Large Diameter Pipes in CO2 Containing Aqueous Media // CORROSION 2003, 16-20 March 2003, San Diego, California. NACE International, 2003. № 03118. Bosch C., Poepperling R.K. Influence of Chromium Contents of 0.5 to 1.0 % on the Corrosion Behavior of Low Alloy Steel for Large Diameter Pipes in CO2 Containing Aqueous Media. CORROSION 2003, 16-20 March 2003, San Diego, California. NACE International, 2003. N 03118. Ali A.E.A., Cioncolini A., Laurence D., Iacovides H. Liquid lead flow-accelerated corrosion testing with the rotating cage set-up: A CFD optimization // Annals of Nuclear Energy. 2022. Vol. 165. № 108620. DOI: 10.1016/j.anucene.2021.108620 Ali A.E.A., Cioncolini A., Laurence D., Iacovides H. Liquid lead flow-accelerated corrosion testing with the rotating cage set-up: A CFD optimization. Annals of Nuclear Energy. 2022. Vol. 165. N 108620. DOI: 10.1016/j.anucene.2021.108620 Nesic S. Effects of Multiphase Flow on Internal CO2 Corrosion of Mild Steel Pipelines // Energy & Fuels. 2012. Vol. 26. № 7. P. 4098-4111. DOI: 10.1021/ef3002795 Nesic S. Effects of Multiphase Flow on Internal CO2 Corrosion of Mild Steel Pipelines. Energy & Fuels. 2012. Vol. 26. N 7, p. 4098-4111. DOI: 10.1021/ef3002795 Ige O.O., Barker R., Hu X. et al. Assessing the influence of shear stress and particle impingement on inhibitor efficiency through the application of in-situ electrochemistry in a CO2-saturated environment // Wear. 2013. Vol. 304. Iss. 1-2. P. 49-59. DOI: 10.1016/j.wear.2013.04.013 Ige O.O., Barker R., Hu X. et al. Assessing the influence of shear stress and particle impingement on inhibitor efficiency through the application of in-situ electrochemistry in a CO2-saturated environment. Wear. 2013. Vol. 304. Iss. 1-2, p. 49-59. DOI: 10.1016/j.wear.2013.04.013 Kumar A., Pacheco J.L., Desai S.K. et al. Effects of Rotating Cage Autoclave Design on Shear Stress and Flow Pattern // CORROSION 2013, 17-21 March 2013, Orlando, Florida. NACE International, 2013. № 2013-2294. Kumar A., Pacheco J.L., Desai S.K. et al. Effects of Rotating Cage Autoclave Design on Shear Stress and Flow Pattern. CORROSION 2013, 17-21 March 2013, Orlando, Florida. NACE International, 2013. N 2013-2294. Liu H., Feng Y., Yao Y. et al. Effect of the 345 °C and 16.5 MPa autoclave corrosion on theoxidation behavior of Cr-coated zirconium claddings in the high-temperature steam // Corrosion Science. 2021. Vol. 189. № 109608. DOI: 10.1016/j.corsci.2021.109608 Liu H., Feng Y., Yao Y. et al. Effect of the 345 °C and 16.5 MPa autoclave corrosion on theoxidation behavior of Cr-coated zirconium claddings in the high-temperature steam. Corrosion Science. 2021. Vol. 189. N 109608. DOI: 10.1016/j.corsci.2021.109608 Zhao Y., Li X., Zhang C. et al. Investigation of the rotation speed on corrosion behavior of HP-13Cr stainless steel in the extremely aggressive oil field environment by using the rotating cage test // Corrosion Science. 2018. Vol.145. P. 307-319. DOI: 10.1016/j.corsci.2018.10.011 Zhao Y., Li X., Zhang C. et al. Investigation of the rotation speed on corrosion behavior of HP-13Cr stainless steel in the extremely aggressive oil field environment by using the rotating cage test. Corrosion Science. 2018. Vol. 145, p. 307-319. DOI: 10.1016/j.corsci.2018.10.011