Ключевые слова

2411-3336

2541-9404

Записки Горного института

Journal of Mining Institute

Санкт-Петербургский горный университет императрицы Екатерины ΙΙ

Empress Catherine II Saint Petersburg Mining University

10.31897/PMI.2022.56

pmi-14688

https://pmi.spmi.ru/pmi/article/view/14688

Геотехнология и инженерная геология

Geotechnical Engineering and Engineering Geology

Manifestation of incompatibility of marine residual fuels: a method for determining compatibility, studying composition of fuels and sediment

Проявление несовместимости судовых остаточных топлив: способ определения совместимости, исследования состава топлив и осадка

Sultanbekov

Radel R.

Cултанбеков

Р. Р.

Sultanbekov

Radel R.

RadelSultanbekov@mail.ru

0000-0002-3192-7680

Санкт-Петербургский горный университет (Россия) Saint Petersburg Mining University (Russia)

Schipachev

Andrey M.

Щипачев

А. М.

Schipachev

Andrey M.

schipachev_am@pers.spmi.ru

0000-0001-6148-6073

Санкт-Петербургский горный университет (Россия) Saint Petersburg Mining University (Russia)

07 11 2022

2022

257 843 852 12 02 2021 26 07 2022 10 11 2022

2022

Р. Р. Cултанбеков, А. М. Щипачев

Radel R. Sultanbekov, Andrey M. Schipachev

Эта статья доступна по лицензии Creative Commons Attribution 4.0 International (CC BY 4.0)

This article is licensed under a Creative Commons Attribution 4.0 International License (CC BY 4.0)

https://pmi.spmi.ru/pmi/article/view/14688

Представлены результаты исследований проблемы активного осадкообразования при смешении остаточных топлив, вызванного проявлением несовместимости. Разработан лабораторный способ определения совместимости и стабильности топлив, позволяющий выявлять количественную характеристику активности осадкообразования. Выполнены лабораторные исследования и обозначены несовместимые компоненты топлив. Проведены испытания для определения показателей качества проб и группового индивидуального состава топлив. Установлены результаты содержания общего и неорганического углерода в полученных осадках с помощью прибора Shimadzu TOC-V SSM 5000A. Определен и рассчитан химический состав на анализаторе LECO CHN-628. Групповой состав входящих в осадок топлив углеводородов изучен с помощью метода газовой хромато-масс-спектрометрии на приборе GCMS-QP2010 Ultra Shimadzu. Для получения дополнительной информации о структурно-групповом составе осадка топлив проведены исследования методом ИК-спектрометрии на ИК-Фурье спектрометре IRAffinity-1. Осуществлен рентгеноструктурный анализ образцов осадка с помощью рентгеновского дифрактометра XRD-7000 Shimadzu, критериями оценки были межплоскостные расстояния d002 и d100, а также размеры кристаллитов Lс и Lа. Выполнен микроструктурный анализ общего осадка методом сканирующей электронной микроскопии. Результаты исследований подтвердили, что на осадкообразование главным образом влияет содержание алканов нормального строения в составе топливной смеси. Разработаны рекомендации по сохранению качества топлив и снижению осадкообразования при хранении и транспортировке.

The results of studying the problem of active sediment formation when mixing residual fuels, caused by manifestation of incompatibility, are presented. A laboratory method has been developed for determining the compatibility and stability of fuels allowing identification of a quantitative characteristic of sediment formation activity. Laboratory studies were performed, and incompatible fuel components were identified. Tests were made to determine the quality indicators of samples and group individual composition of fuels. Results on the content of total and inorganic carbon in the obtained sediments were determined using Shimadzu TOC-V SSM 5000A. Chemical composition was determined and calculated on LECO CHN-628 analyser. Group composition of hydrocarbon fuels contained in the sediment was studied by gas chromato-mass spectrometry on GCMS-QP2010 Ultra Shimadzu. To obtain additional information on the structural group composition of fuel sediment, IR spectrometry was performed on IR-Fourier spectrometer IRAffinity-1. X-ray diffraction analysis of sediment samples was made using X-ray diffractometer XRD-7000 Shimadzu; interplanar distances d002 and d100 as well as Lс and Lа crystallite sizes served as the evaluation criteria. Microstructural analysis of total sediment was performed by scanning electron microscopy. The results of the research confirmed that the content of normal alkanes in the fuel mixture mainly affects sediment formation. Recommendations were drawn on preserving the quality of fuels and reducing sediment formation during storage and transportation.

Ключевые слова судовые остаточные топлива несовместимость стабильность хранение общий осадок групповой и элементный состав

Keywords marine residual fuels incompatibility stability storage total sediment group and elemental composition

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